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Magnetization study of the kinetic arrest of martensitic transformation in as-quenched Ni52.2Mn34.3In13.5 melt spun ribbons

Published online by Cambridge University Press:  05 March 2013

F.M. Lino-Zapata ,
J.L. Sánchez Llamazares ,
D. Ríos-Jara ,
A.G. Lara-Rodríguez  and
T. García-Fernández
F.M. Lino-Zapata
Affiliation:
Instituto Potosino de Investigación Científica y Tecnológica, Camino a la Presa San José 2055 Col. Lomas 4ª, San Luis Potosí, S.L.P. 78216, México.
J.L. Sánchez Llamazares
Affiliation:
Instituto Potosino de Investigación Científica y Tecnológica, Camino a la Presa San José 2055 Col. Lomas 4ª, San Luis Potosí, S.L.P. 78216, México.
D. Ríos-Jara
Affiliation:
Instituto Potosino de Investigación Científica y Tecnológica, Camino a la Presa San José 2055 Col. Lomas 4ª, San Luis Potosí, S.L.P. 78216, México.
A.G. Lara-Rodríguez
Affiliation:
Instituto de Investigaciones en Materiales, UNAM, Circuito Exterior s/n, Ciudad Universitaria, México D.F. 04510, México.
T. García-Fernández
Affiliation:
Universidad Autónoma de la Ciudad de México, Prolongación San Isidro 151,Col. San Lorenzo Tezonco, México DF, C.P. 09790, México
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Abstract

The kinetic arrest of martensitic transformation (MT) has been observed in as-solidified Ni52.2Mn34.3In13.5 melt spun ribbons. The main characteristics of this unusual field-induced magneto-structural phenomenon have been determined through a dc magnetization study. The sample studied was fabricated by rapid solidification using the melt spinning technique at a high quenching rate of 48 ms-1. At room temperature, it is a single phase austenite (AST) with the bcc B2-type crystal structure and Curie temperature of TCA=285 K. With decreasing temperature, the austenite phase transforms into the martensite phase (MST) with TCM≈185 K at a starting martensitic transition temperature of MS=275 K. A moderate but progressive kinetic arrest of the AST to MST transformation has been observed for magnetic field values above H=10 kOe and was studied up to Hmax= 90 kOe. The metastable character of the non-equilibrium field-cooled state is revealed by the decreasing behavior of the saturation magnetization under a large magnetic field of 50 kOe after temperature cycling from 10 K to 150 K. The total magnetization difference Δσ between the zero field-cooling and field-cooling pathways of the temperature dependence of magnetization shows irreversible and reversible components and the former decreases with decreasing temperature.

Keywords

Magnetic propertiesmicrostructurerapid solidification
Type
Articles
Information
MRS Online Proceedings Library (OPL) , Volume 1485: Symposium 7D – Advanced Structural Materials—2012 , 2012 , pp. 149 - 154
Copyright
Copyright © Materials Research Society 2013 

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References

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