Hostname: page-component-586b7cd67f-g8jcs Total loading time: 0 Render date: 2024-11-23T20:40:50.902Z Has data issue: false hasContentIssue false

Magnetic Properties of Nd-Fe-B-M (M=Si, C) Bulk Nanocomposite Magnets Prepared by the Spark Plasma Sintering Method

Published online by Cambridge University Press:  26 February 2011

Tomokazu Fukuzaki
Affiliation:
[email protected], Tokyo University of Sicence, Polyscale Technology Research Center, 2641, Ymazaki, Noda-shi, Chiba-ken, 278-8510, Japan
Keisuke Tanaka
Affiliation:
[email protected], Tokyo University of Science, Department of Materials Science and Technology, 2641, Yamazaki, Noda-shi, Chiba-ken, 278-8510, Japan
Kazue Nishimoto
Affiliation:
[email protected], Tokyo University of Science, Department of Materials Science and Technology, 2641, Yamazaki, Noda-shi, Chiba-ken, 278-8510, Japan
Yuji Muro
Affiliation:
[email protected], Tokyo University of Science, Department of Physics, 2641, Yamazaki, Noda-shi, Chiba-ken, 278-8510, Japan
Keishi Nishio
Affiliation:
[email protected], Tokyo University of Science, Department of Materials Science and Technology, 2641, Yamazaki, Noda-shi, Chiba-ken, 278-8510, Japan
Ryuji Tamura
Affiliation:
[email protected], Tokyo University of Science, Department of Materials Science and Technology, 2641, Yamazaki, Noda-shi, Chiba-ken, 278-8510, Japan
Get access

Abstract

We have prepared Nd2Fe14B/Fe3B bulk nanocomposite magnets at the compositions of Nd4Fe77.5B18.5-xMx (M=Si, C) by substitution of other elements M for B. For the sample substituted with 1 at.%Si and sintered at 600 oC, the coercivity exhibits the highest value of 227 kA/m. It has also been found that the grain sizes of the Nd2Fe14B and the Fe3B phases depend on the ramp-up time and the reduction of the grain size leads to an increase of the coercivity. On the other hand, the samples substituted with C exhibit soft magnetic behaviors, which is attributed to the suppression of the precipitation of the Nd2Fe14B hard magnetic phase.

Type
Research Article
Copyright
Copyright © Materials Research Society 2008

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1. Saito, T., J. Mater. Res., Vol. 19, No. 9, 2730, (2004)10.1557/JMR.2004.0358Google Scholar
2. Saito, T., Takeuchi, T., and Kageyama, H., IEEE Trans. Magn., Vol. 40, No. 4, 2880, (2004)10.1109/TMAG.2004.834211Google Scholar
3. Coehoorn, R., Mooij, D. B. de, and Waard, C. de, J. Magn. Magn. Matter., Vol. 80, 101, (1981)10.1016/0304-8853(89)90333-8Google Scholar
4. Kneller, E. F. and Hawig, R., IEEE Trans. Magn., Vol. 27, 3588, (1991)10.1109/20.102931Google Scholar