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Laser-Assisted Atom Probe Analysis of Bulk Insulating Ceramics

Published online by Cambridge University Press:  31 January 2011

Tadakatsu Ohkubo ,
Yimeng M. Chen ,
Masaya Kodzuka ,
Fang Li ,
Keiichiro Oh-ishi  and
Kazuhiro Hono
Tadakatsu Ohkubo
Affiliation:
[email protected], National Institute for Materials Science, Magnetic Materials Center, Tsukuba, Japan
Yimeng M. Chen
Affiliation:
[email protected], University of Tsukuba, Graduate School of Pure and Applied Sciences, Tsukuba, Japan
Masaya Kodzuka
Affiliation:
[email protected], University of Tsukuba, Graduate School of Pure and Applied Sciences, Tsukuba, Japan
Fang Li
Affiliation:
[email protected], National Institute for Materials Science, Magnetic Materials Center, Tsukuba, Japan
Keiichiro Oh-ishi
Affiliation:
[email protected], National Institute for Materials Science, Magnetic Materials Center, Tsukuba, Japan
Kazuhiro Hono
Affiliation:
[email protected], National Institute for Materials Science, Magnetic Materials Center, Tsukuba, Japan
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Abstract

A Yb:KGW femtosecond laser (400 fs) with 3rd and 4th harmonic generators (wavelength = 343 and 258 nm) was adopted to a locally built 3DAP instrument to assist field evaporation from ceramics tips that were bonded on tungsten wire. Using this setting, we have demonstrated that quantitative atom probe tomography is possible from Y2O3-ZrO2-MgAl2O4, (Ce,Y)O2, Li(Co,Ni,Mg,Al)O2 sintered bulk ceramics, which are all insulators.

Keywords

ceramicinsulatornanostructure
Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 1231: Symposium NN – Advanced Microscopy and Spectroscopy Techniques for Imaging Materials with High Spatial Resolution , 2009 , 1231-NN02-09
Copyright
Copyright © Materials Research Society 2010

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