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Influence of Cyclodextrin in the Synthesis of Magnetite

Published online by Cambridge University Press:  01 February 2011

L. A. Cobos Cruz ,
C. A. Martínez Perez ,
A Martínez Villafañe ,
J. A. Matutes Aquino ,
J. R. Farias Macilla  and
P. E. García Casillas
L. A. Cobos Cruz
Affiliation:
Instituto de Ing. y Tecnología, Universidad Autónoma de Cd. Juárez, Cd. Juárez Chih., México
C. A. Martínez Perez
Affiliation:
Instituto de Ing. y Tecnología, Universidad Autónoma de Cd. Juárez, Cd. Juárez Chih., México
A Martínez Villafañe
Affiliation:
Centro de Investigaciones en Materiales Avanzados, Chihuahua, Chih., México
J. A. Matutes Aquino
Affiliation:
Centro de Investigaciones en Materiales Avanzados, Chihuahua, Chih., México
J. R. Farias Macilla
Affiliation:
Centro de Investigaciones en Materiales Avanzados, Chihuahua, Chih., México
P. E. García Casillas
Affiliation:
Instituto de Ing. y Tecnología, Universidad Autónoma de Cd. Juárez, Cd. Juárez Chih., México
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Abstract

Cyclodextrin (CD) has been studied intensively due to its ability to form inclusion complexes with a variety of guest molecules in the solid state. A few studies have paid attention to the use of CD to facilitate the synthesis of inorganic nanoparticles. In this work the synthesis of magnetite (M) is made in the presence of CD. The particle size of the inorganic material is controlled by the presence of CD, in which spherical particles of few nanometers are grown. The synthesis of Fe3O4 (M) in the presence of α-cyclodextrin (α-CD) and β-cyclodextrin (βCD) is described. The formation of an M-CD complex is studied in both cases by Fourier transform infrared spectroscopy (FT-IR) in order to elucidate the chemical bonding of the complex. The morphology and size of the particles are determined by Field Emission Scanning Electron Microscopy (FESEM) and software. X-ray diffraction (XRD) is used to confirm the formation of magnetite.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 1243: Symposium 5 – Advanced Structural Materials , 2009 , 11
Copyright
Copyright © Materials Research Society 2010

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References

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