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Genesis and Growth of Nanoparticles during Sol-Gel Synthesis

Published online by Cambridge University Press:  01 February 2011

Nan Yao
Affiliation:
Department of Chemical Engineering, Hong Kong University of Science and Technology, Clear Water Bay, Kowloon, Hong Kong, P. R. China
King Lun Yeung*
Affiliation:
Department of Chemical Engineering, Hong Kong University of Science and Technology, Clear Water Bay, Kowloon, Hong Kong, P. R. China
Guoxing Xiong*
Affiliation:
State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, P. O. Box 110, Dalian 116023, P. R. China
Shishan Sheng
Affiliation:
State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, P. O. Box 110, Dalian 116023, P. R. China
*
* Corresponding authors
* Corresponding authors
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Abstract

In situ observation of the genesis and growth of silica-alumina structures during the sol-gel process has been carried out. Although the gross structure of the gel network is kinetically stabilized, in situ AFM study reveals that at nanometer scale, the internal structure of the gel is dynamic as shown by the rich and complex morphological transformations.

Type
Research Article
Copyright
Copyright © Materials Research Society 2004

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References

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