Hostname: page-component-cd9895bd7-8ctnn Total loading time: 0 Render date: 2024-12-27T01:55:51.658Z Has data issue: false hasContentIssue false

Frequency Specific Characterization of Very Soft Polymeric Materials Using Nanoindentation Testing

Published online by Cambridge University Press:  17 March 2011

Nicolas Conte
Affiliation:
University of Tennessee, Department of Materials Science and Engineering, Knoxville, TN 37996, USA
Vincent Jardret
Affiliation:
MTS Nano Instruments Innovation Center, 1001 Larson Drive, Oak Ridge, TN 37830, USA
Get access

Abstract

Polymer thin films and surfaces play a major role in the functionality of many components in the microelectronic and automotive industries. The characterization of their mechanical properties at a nanometer scale remains a technological challenge. Instrumented indentation testing with frequency-specific dynamic analysis provides access to viscoelastic measurement of near surface properties of polymeric materials. Development of biomaterials for tissue replacement raises the interest for testing polymers with storage modulus of less than 1 MPa. The development of specific testing methodologies with improved accuracy and precision for evaluating very soft polymeric materials are presented in this work. Results at various frequencies for polyurethane and polydimethylsilane using both Berkovich and Flat punch geometries are compared.

Type
Research Article
Copyright
Copyright © Materials Research Society 2002

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1- Pethica, J. B. and Oliver, W. C. in Thin Films: Stresses and Mechanical Properties I, Mat. Res. Soc. Symp. Proc., 130, (1989).Google Scholar
2- Oliver, W. C. and Pharr, G. M., J. Mat. Res., 7, (1992).Google Scholar
3- Hay, J. L. and Pharr, G. M., ASM Handbook, 8, (2000).Google Scholar
4- Oliver, W. C. and Pethica, J. B., U. S. Patent No. 4848141.Google Scholar
5- Lucas, B. N., Ph. D. Dissertation, The University of Tennessee, Knoxville, (1997).Google Scholar
6- Loubet, J-L., Lucas, B. N. and Oliver, W. C., Conference Proceedings: International Workshop on Instrumented Indentation, NIST Spec. Publ., 896, San Diego, CA, April 22-23, 3134 (1995).Google Scholar
7- Lucas, B. N., Oliver, W. C. and Swindeman, J.E., Mat. Res. Soc. Symp. Proc., 522, (1998).Google Scholar
8- Lucas, B. N., Oliver, W. C., Pharr, G. M. and Loubet, J-L., Mat. Res. Soc. Symp. Proc., 436, (1996).Google Scholar