Hostname: page-component-cd9895bd7-q99xh Total loading time: 0 Render date: 2024-12-27T02:05:49.906Z Has data issue: false hasContentIssue false
  • English
  • Français

Flame Spray Pyrolysis of Electrode Materials for Energy Applications

Published online by Cambridge University Press:  08 April 2015

Paul I. Dahl ,
Magnus S. Thomassen ,
Luis C. Colmenares ,
Alejandro O. Barnett ,
Scott Lomas ,
Per E. Vullum ,
Sidsel M. Hanetho  and
Tommy Mokkelbost
Paul I. Dahl*
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
Magnus S. Thomassen
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
Luis C. Colmenares
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
Alejandro O. Barnett
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
Scott Lomas
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
Per E. Vullum
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
Sidsel M. Hanetho
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
Tommy Mokkelbost
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
*
*Corresponding author: [email protected], +47-98243955
Get access

Abstract

Flame spray pyrolysis (FSP) was applied to produce nanopowders of Ti1-xMxO2 and Sn1-xMxO2, where x = 0.05 and M = Nb/Sb, for use as catalyst support materials in PEM fuel cells/ electrolysers. FSP powders in the SnO2-IrO2 system were produced for the same applications. Homogenous particle size distribution (5-20 nm) was demonstrated by TEM, supported by BET and XRD analysis. Whereas two polymorphs were indicated for the Ti-based oxides, the Sb/Nb-doped SnO2 powders were single phase. FSP powders of Mn3O4 intended for supercapacitors were produced and the influence of the precursor/solvent mixtures on the physical and electrochemical properties evaluated.

Keywords

flame synthesisoxidenanoscale
Type
Articles
Information
MRS Online Proceedings Library (OPL) , Volume 1747: Symposium HH – Flame and High-Temperature Synthesis of Functional Nanomaterials—Fundamentals and Applications , 2015 , mrsf14-1747-hh05-10
Copyright
Copyright © Materials Research Society 2015 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

Teoh, W.Y., Amal, R., Madler, L., Nanoscale, 2010. 2(8): p. 1324–1347.CrossRefGoogle Scholar
Sharma, S., Pollet, B.G., Journal of Power Sources, 2012. 208: p. 96–119.CrossRefGoogle Scholar
Rabis, A., Rodriguez, P., Schmidt, T.J., Acs Catalysis, 2012. 2(5): p. 864–890.CrossRefGoogle Scholar
Takasaki, F., Matsuie, S., Takabatake, Y., Noda, Z., Hayashi, A., Shiratori, Y., Ito, K., Sasaki, K., Journal of the Electrochemical Society, 2011. 158(10): p. B1270–B1275.CrossRefGoogle Scholar
Tsukatsune, T., Takabatake, Y., Noda, Z., Hayashi, A., Sasaki, K., Polymer Electrolyte Fuel Cells 10, Pts 1 and 2, 2013. 58(1): p. 1251–1257.Google Scholar
Kanda, K., Noda, Z., Nagamatsu, Y., Higashi, T., Taniguchi, S., Lyth, S. M., Hayashi, A., Sasaki, K., ECS Electrochemistry Letters, 2014. 3(4): p. F15–F18.CrossRefGoogle Scholar
Teleki, A., Bjelobrk, N., Pratsinis, S.E., Sensors and Actuators B: Chemical, 2008. 130(1): p. 449–457.CrossRefGoogle Scholar
Grossmann, K., Kovacs, K. E., Pham, D. K., Madler, L., Barsan, N., Weimar, U., Sensors and Actuators B-Chemical, 2011. 158(1): p. 388–392.CrossRefGoogle Scholar
Madler, L., Roessler, A., Pratsinis, S. E., Sahm, T., Gurlo, A., Barsan, N., Weimar, U., Sensors and Actuators B-Chemical, 2006. 114(1): p. 283–295.CrossRefGoogle Scholar
Zhang, S.W., Chen, G.Z., Energy Materials: Materials Science and Engineering for Energy Systems, 2008. 3(3): p. 186–200.CrossRefGoogle Scholar
Karthikeyan, J., Berndt, C. C., Tikkanen, J., Wang, J. Y., King, A. H., Herman, H., Nanostructured Materials, 1997. 8(1): p. 61–74.CrossRefGoogle Scholar
Tikkanen, J., Gross, K. A., Berndt, C. C., Pitkanen, V., Keskinen, J., Raghu, S., Rajala, M., Karthikeyan, J., Surface & Coatings Technology, 1997. 90(3): p. 210–216.CrossRefGoogle Scholar
Liu, G., Yue, R. L., Jia, Y., Ni, Y., Yang, J., Liu, H. D., Wang, Z., Wu, X. F., Chen, Y. F., Particuology, 2013. 11(4): p. 454–459.CrossRefGoogle Scholar
Kim, J.H., Choi, S. H., Son, M. Y., Kim, M. H., Lee, J. K., Kang, Y. C., Ceramics International, 2013. 39(1): p. 331–336.CrossRefGoogle Scholar
Ernst, F.O., Kammler, H. K., Roessler, A., Pratsinis, S. E., Stark, W. J., Ufheil, J., Novak, P., Materials Chemistry and Physics, 2007. 101(2-3): p. 372–378.CrossRefGoogle Scholar
Marshall, A., Børresen, B. Hagen, G., Tsypkin, M., Tunold, R., Electrochimica Acta, 2006. 51(15): p. 3161–3167.CrossRefGoogle Scholar