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Published online by Cambridge University Press: 15 February 2011
A highly detailed x-ray photoelectron diffraction data set has been acquired for crystalline Cu(001). The data set for bulk Cu 3p emission encompasses a large k-space volume (k=3–10 Å-1) with sufficient energy and angular sampling to monitor the continuous variation of diffraction intensities. The evolution of back-scattered intensity oscillations is visualized by energy and angular slices of this ‘volume’ data set. Large diffractyyion data sets such as this will provide rigorous experimental tests of real-space reconstruction algorithms and multiple-scattering simulations.