Hostname: page-component-78c5997874-j824f Total loading time: 0 Render date: 2024-11-19T06:23:50.867Z Has data issue: false hasContentIssue false

Comparison of Performance of an Analytical Electron Microscope at 300 and 100 kV*

Published online by Cambridge University Press:  25 February 2011

J. Bentley
Affiliation:
Metals and Ceramics Division, Oak Ridge National Laboratory, Oak Ridge, TN 37831
E. A. Kenik
Affiliation:
Metals and Ceramics Division, Oak Ridge National Laboratory, Oak Ridge, TN 37831
P. Angelini
Affiliation:
Metals and Ceramics Division, Oak Ridge National Laboratory, Oak Ridge, TN 37831
A. T. Fisher
Affiliation:
Metals and Ceramics Division, Oak Ridge National Laboratory, Oak Ridge, TN 37831
P. S. Sklad
Affiliation:
Metals and Ceramics Division, Oak Ridge National Laboratory, Oak Ridge, TN 37831
G. L. Lehman
Affiliation:
Oak Ridge Associated Universities, Oak Ridge, TN 37831
J. A. Horton Jr.
Affiliation:
Metals and Ceramics Division, Oak Ridge National Laboratory, Oak Ridge, TN 37831
Get access

Abstract

Preliminary results on the performance of an analytical electron microscope (AEM) operating at 300 kV have been obtained and compared with the performance at 100 kV. Some features of the anticipated improvements for transmission electron microscopy (TEM) imaging, convergent beam electron diffraction (CBED), energy dispersive X-ray spectroscopy (EDS), and electron energy loss spectroscopy (EELS) have been studied from the aspect of materials science applications. The electron microscope used was a Philips EM430T operated with a LaB6 cathode and equipped with EDAX 9100/70 EDS and Gatan 607 EELS systems.

Type
Research Article
Copyright
Copyright © Materials Research Society 1985

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

Footnotes

*

Research sponsored by the Division of Materials Sciences, . S. Department of Energy under contract DE-ACO5-840R21400 with Martin Marietta Energy Systems, Inc.

References

1. Hirsch, P. B., Howie, A., Nicholson, R. B., Pashley, D.W. and Whelan, M.J., Electron Microscopy of Thin Crystals, Butterworths, London, 1965.Google Scholar
2. Spence, J. C. H., Experimental High-resolution Electron Microscopy, Oxford University Press, New York, 1981.10.1063/1.2914772CrossRefGoogle Scholar
3. Steeds, J. W., in: Introduction to Analytical Electron Microscopy, eds. Hren, J. J., Goldstein, J. I. and Joy, D. C., Plenum, New York, 1979, p.387.10.1007/978-1-4757-5581-7_15CrossRefGoogle Scholar
4. Zaluzec, N. J., Taylor, A., Ryan, E. A. and Philippides, A., in: Proc. 7th Int. Conf. on High Voltage Electron Microscopy, eds. Fisher, R.M., Gronsky, R. and Westmacott, K.H., Lawrence Berkeley Laboratory Report LBL-16031, 1983, p.79.Google Scholar
5. Zaluzec, N. J., in: Introduction to Analytical Electron Microscopy, eds. Hren, J. J., Goldstein, J.I. and Joy, D.C., Plenum, New York, 1979, p.121.10.1007/978-1-4757-5581-7_4CrossRefGoogle Scholar
6. Bentley, J., Zaluzec, N. J., Kenik, E. A. and Carpenter, R. W., Scanning Electron Microscopy/1979/II, SEM Inc., AMF O'Hare (Chicago), p.581.Google Scholar
7. Steel, E. and Newbury, D. E., in: Analytical Electron Microscopy 1984, eds. Williams, D. B. and Joy, D.C., San Francisco Press, San Francisco.Google Scholar
8. Angelini, P. and Bentley, J.,in: 42nd Ann. Proc. Electron Microscopy Soc. Amer., ed. Bailey, G.W., San Francisco Press, San Francisco, 1984, p.582.Google Scholar
9. Maher, D. M., in: Introduction to Analytical Electron Microscopy, eds. Hren, J. J., Goldstein, J.I. and Joy, D.C., Plenum, New York, 1979, p.259.10.1007/978-1-4757-5581-7_9CrossRefGoogle Scholar
10. Bentley, J., Lehman, G. L. and Sklad, P. S., in: 40th Ann. Proc. Electron Microscopy Soc. Amer., ed. Bailey, G.W., Claitors, Baton Rouge, 1982, p.496.Google Scholar
11. Analytical Electron Microscopy 1981, ed. Geiss, R.H., San Francisco Press, San Francisco, 1981.Google Scholar
12. Analytical Electron Microscopy 1984, eds. Williams, D.B. and Joy, D.C., San Francisco Press, San Francisco, 1985.Google ScholarPubMed