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Chemical synthesis of nanoparticles for artificial pinning centers in YBCO coated conductors

Published online by Cambridge University Press:  01 February 2011

Srivatsan Sathyamurthy
Affiliation:
Oak Ridge National Laboratory, Oak Ridge, TN 37831
Keith J. Leonard
Affiliation:
Oak Ridge National Laboratory, Oak Ridge, TN 37831
M. Parans Paranthaman
Affiliation:
Oak Ridge National Laboratory, Oak Ridge, TN 37831
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Abstract

Ceria nanoparticles were prepared using a solution based approach using cerium (III) acetate as a starting material and cetyltrimethylammonium hydroxide (CTAOH) as a precipitating agent and surfactant. The presence of the surfactant CTAOH helps prevent agglomeration of the nanoparticles. Using X-ray diffraction (XRD) and high resolution transmission electron microscopy (HRTEM), the particle size was determined to be 3.5 – 4 nm. The structure and properties of these CeO2 nanoparticles have been analyzed.

Type
Research Article
Copyright
Copyright © Materials Research Society 2005

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References

1 Macmanus-Driscoll, J.L, Foltyn, S.R, Jia, Q.X, Wang, H, Serquis, A, Civale, L, Maiorov, B, Hawley, M.E, Maley, M.P and Peterson, D.E 2004 Nature Materials 3 439 (2004).Google Scholar
2 Amit, Goyal et al. Results presented at the Annual Peer Review of the DOE Superconductivity Program, Washington DC (2004).Google Scholar
3 Trovarelli, A Catal. Rev. Sci. Eng. 38 439 (1996)Google Scholar
4 Steele, B.C.H Nature 414 345 (2001).Google Scholar
5 Yu, X.J, Xie, P.B, and Su, Q.D Phys. Chem. Chem. Phys. 3 5266 (2001).Google Scholar
6 Guillou, N, Nistor, L.C, Fuess, H, Hahn, H Nanostructured Materials 8 545 (1997).Google Scholar
7 Zheng, F, Jin, Q, and Chan, S-W J. Appl. Phys. 95 4319 (2004).Google Scholar
8 Czerwinski, F and Szpunar, J.A J. Sol-gel Sci. Tech. 9 103 (1997).Google Scholar
9 Wang, Z.L and Feng, X J. Phys. Chem. B 107 13563 (2003).Google Scholar
10 Zhitomirsky, I and Petric, A Ceram. Int. 27 149 (2001).Google Scholar
11 Sathyamurthy, S, Leonard, K.J, Debastani, R, and Paranthaman, M, Nanotechnology (submitted)Google Scholar
12 Leonard, K.J, Sathyamurthy, S, and Paranthaman, M, Chemistry of Materials (submitted)Google Scholar
13 Hingorani, S, Pillai, V, Kumar, P, Multani, M.S, and Shah, D.O Mater. Res. Bull. 28 1303 (1993).Google Scholar
14 Yin, L, Wang, Y, Pang, G, Koltypin, Y, and Gedanken, A J. Colloid and Interface Science 246 78 (2002).Google Scholar
15 Yu, S-H, Colfen, H, and Fischer, A Colloids and Surfaces A 243 49 (2004).Google Scholar
16 Masui, T, Fujiwara, K, Machida, K, and Adachi, G Chem. Mater. 9 2197 (1997).Google Scholar