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X-Ray Diffraction for Nondestructive Characterization of Polycrystalline Materials

Published online by Cambridge University Press:  21 February 2011

C. O. Ruud
Affiliation:
The Pennsylvania State University, 159 Materials Research Laboratory, University Park, PA 16802.
S. D. Weedman
Affiliation:
The Pennsylvania State University, 159 Materials Research Laboratory, University Park, PA 16802.
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Abstract

X-ray diffraction has long been the mainstay for materials characterization in the laboratory. This characterization includes the determination of phase composition, residual stress, microstrain, grain size, and crystallographic texture of polycrystalline metals, ceramics, and minerals. The analytical capabilities of XRD techniques have been expanded recently by the application of computer control to data collection and processing. These capabilities include the identification of irregularities in metals and ceramics that are caused by processing and fatigue damage, as well as the apriori prediction of processing anomolies. While the above applications have been largely restricted to the laboratory, the possibility for exploitation of the nondestructive nature of x-ray diffraction for inprocess evaluation of materials is now being realized. The availability of computer-controlled position-sensitive x-ray detectors can now provide rapid, non-contacting, in-process interrogation of materials. The examples of nondestructive characterization illustrated in this paper will be those that can be used for process control and/or damage assessment.

Type
Research Article
Copyright
Copyright © Materials Research Society 1989

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References

1. Ruud, C. O., Ind. Res. and Dev. 84–87, (January, 1983).Google Scholar
2. Ruud, C. O., DiMascio, P. S., and Snoha, D. J., in Adv. in X-Ray Anal, 21, (Plenum Press, New York, 1984), pp. 273282.Google Scholar
3. Ruud, C. O., Nondestructive Methods for Material Property Determination, edited by Ruud, C. O. and Green, R. E. Jr,. (Plenum Press, New York, 1984), Vol.1, pp. 2137.Google Scholar
4. Personal communication, Doxbeck, M.A, Benet Weapons Laboratory, Watervliet, New York, May, 1986.Google Scholar
4. Cullity, B. D., Elements of X-Ray Diffraction, Second Edition (Addison-Wesley, Reading, MA, 1978).Google Scholar
6. SAE, “Residual Stress Measurement by X-Ray Diffraction - J784a,” Soc. of Auto. Eng., Warrendale, PA (1971).Google Scholar
7. Delhez, R., de Keijser, Th. H., and Mittemeijer, E. J., Surface Engineering., 3 331342 (1987).Google Scholar
8. Lo, C. F., Kamide, H., Mayo, W. E., and Weissman, S., in press.Google Scholar
9. Khatri, R. P., Pangborn, R. N., Cook, T. S., and Roberts, M., Jour. of Mater. Sci. 21, 511521 (1986).Google Scholar
10. Kurita, M., Ihara, I., Shinbo, M., and Koguchi, H., Jour. of Testing and Eval. 33–39 (January, 1986).Google Scholar