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Synthesis and characterization of colloidal titania nanoparticles

Published online by Cambridge University Press:  01 February 2011

Ana-Lilia Díaz-Fonseca  and
Juan-Carlos Cheang-Wong
Ana-Lilia Díaz-Fonseca
Affiliation:
[email protected], Instituto de Física, Universidad Nacional Autónoma de México, A.P. 20-364, México, D.F., 01000, Mexico
Juan-Carlos Cheang-Wong
Affiliation:
[email protected], Instituto de Física, Universidad Nacional Autónoma de México, A.P. 20-364, México, D.F., 01000, Mexico
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Abstract

Spherical submicrometer-sized titanium dioxide (TiO2 or titania) particles were prepared by the sol-gel method from hydrolysis and condensation of titanium alkoxide using different basic catalysts in ethanol/acetonitrile at different annealing temperatures. A systematic study was performed in order to determine the effect on the particle size and shape of the different reagents. Subsequently, they were deposited onto silicon wafers, in order to form a monolayer of TiO2 monodisperse particles. The titania particles were characterized by scanning electron microscopy to determine size and shape, and by X-ray diffraction to find their crystal structure.

Keywords

colloidsol-gelnanostructure
Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 1074: Symposium I – Synthesis and Metrology of Nanoscale Oxides and Thin Films , 2008 , 1074-I10-24
Copyright
Copyright © Materials Research Society 2008

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References

REFERENCES

1. Diebold, U. Surf. Sci. Reports 48, 53 (2003).Google Scholar
2. Benyagoub, A. Loffler, S. Rammensee, M. and Klaumünzer, S., Nucl. Instr. and Meth. B 65, 228 (1992).Google Scholar
3. Cheang-Wong, J.C., Radiation Effects and Defects in Solids 162, 247 (2007).Google Scholar
4. Dillen, T. van, Polman, A. Fukarek, W. Blaaderen, A. Van, Appl. Phys. Lett. 78, 910 (2001).Google Scholar
5. Cheang-Wong, J.C., Morales, U. Reséndiz, E., Oliver, A. Rodríguez-Fernández, L., J. of Non-Cryst. Sol. 353, 1925 (2007).Google Scholar
6. Mine, E. Hirose, M. Nagao, D. Kobayashi, Y. Konno, M. J. Colloid Interface Sci. 291, 162 (2005).Google Scholar
7. Brinker, C.J. and Scherer, G.W. Sol–Gel Science (Academic Press, New York, 1990).Google Scholar
8. Sugimoto, T. “Mechanisms of Nucleation and Growth of Monodispersed Particles” in Encyclopedia of Surface and Colloid Science (Marcel Dekker Inc., 2002).Google Scholar
9. Bradley, D.C. Adv. Chem. Ser., 23, 10 (1959).Google Scholar
10. Sugimoto, T. Zhou, X. Muramatsu, A. J. Colloid Interface Sci 252, 339 (2002).Google Scholar