Hostname: page-component-78c5997874-m6dg7 Total loading time: 0 Render date: 2024-11-19T07:15:29.218Z Has data issue: false hasContentIssue false

Structural and Magnetic X-RAY Scattering Measurements of Epitaxial Dy thin Films

Published online by Cambridge University Press:  26 February 2011

Michael F. Toney
Affiliation:
IBM Research Division, Almaden Research Center, 650 Harry Road, San.Tose, California 95120-6099.
David G. Wiesler
Affiliation:
IBM Research Division, Almaden Research Center, 650 Harry Road, San.Tose, California 95120-6099.
Brent D. Hermsmeier
Affiliation:
IBM Research Division, Almaden Research Center, 650 Harry Road, San.Tose, California 95120-6099.
Robin F. Farrow
Affiliation:
IBM Research Division, Almaden Research Center, 650 Harry Road, San.Tose, California 95120-6099.
Get access

Abstract

We report structural and magnetic X-ray scattering measurements of a 2000Å thick Dy film, sandwiched by LaF3 films on a GaAs(111) substrate. The structure was grow by molecular beam epitaxy with the c-axis of the Dy parallel to the LaF3 c-axis and GaAs[111] axis. For the magnetic X-ray scattering, we used a polarization analyzer and an X-ray energy near the Dy L111 absorption edge. ∆t this energy there is a resonant enhancement in the magnetic scattering intensity, and we obtained ≃-50 counts per second in the magnetic diffraction peaks.

Between 85 and 179K, bulk Dy forms a helical antiferromagnetic structure, and below 85K, it transforms into a ferromagnet. We find that the c-axis lattice constant of the Dy film has a similar temperature dependence to bulk Dy from room temperature to about 110K, but below this, the film behaves differently from bulk and is strained. The temperature dependence of the turn-angle in the helical antiferromagnetic state is similar to bulk, although a weaker dependence is observed below ∼1 10K due to magnetoelastic effects. Surprisingly, the magnetic coherence length (≃310Å) is significantly shorter than the structural coherence length (≃730Å). The transition to ferromagnetic ordering at 86K exhibits temperature hysteresis as is evident in the structural and magnetic X-ray data and in SQUID magnetometry data. We believe this hysteresis arises from a combination of the strain-energy barrier accompanying the transition and magnetic inhomogeneities in the film.

Type
Research Article
Copyright
Copyright © Materials Research Society 1992

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1. Erwin, R.W., Rhyne, J.J., Salamon, M.B., Borchers, J., Sinha, S., Du, R., Cunningham, I.E., and Flynn, C.P., Phys. Rev. B 35, 6808 (1987).CrossRefGoogle Scholar
2. Rhyne, J.J., Erwin, R.W., Borchers, J., Salamon, M.B., Du, R., and Flynn, C.P., Physica B 159, 111 (1989).CrossRefGoogle Scholar
3. Kwo, J., in Thin Film Growth Techniques for Low Dimensional Siructures, edited by Farrow, R.F.C., Parkin, S.S.P., Dobson, P.I., and Neave, I.H. (Plenum, New York, 1989), p. 337.Google Scholar
4. Farrow, R.F.C., Parkin, S.S.P., Lang, M., and Roche, K.P., Mat. Res. Soc. Symp. 103, 205 (1988).CrossRefGoogle Scholar
5. Farrow, R.F.C., Parkin, S.S.P., and Speriosu, V.S., J. Appl. Phys. 64, 5315 (1988).Google Scholar
6. Farrow, R.F.C., Parkin, S.S.P., Speriosu, V.S., Bezinge, A., and Segmuller, A.P., Mat. Res. Soc. Symp. 151, 203 (1989).CrossRefGoogle Scholar
7. Farrow, R.C.F., Toney, M.F., llermsmeier, B.D., Parkin, S.S.P., and Wiesler, D.G., J. Appl. Phys., in press (1991).Google Scholar
8. Specht, E.D., Mak, A., Peters, C., Sutton, M., Birgeneau, R.J., D'Amico, K.L., Moncton, D.E., Nagler, S.E., and Horn, P.M., Z. Phys. 11 69, 347 (1987).CrossRefGoogle Scholar
9. lsaacs, E.D., McWhan, D.B., Siddons, D.P., llastings, I.B., and Gibbs, D., Phys. Rev. B 40, 9336 (1989).Google Scholar
10. Gibbs, D.B., Harshman, D.R., lsaacs, E.D., McWhan, D.B., Mills, D., and Vettier, C., Phys. Rev. Lett. 61, 1241 (1988).CrossRefGoogle Scholar
11. Gibbs, D.B., Physica B 159, 145 (1989).Google Scholar
12. Darnell, F.J., Phys. Rev. 130, 1825 (1963).CrossRefGoogle Scholar
13. Clark, A.E., DeSavage, B.F., and Bozorth, R., Phys. Rev. 138, A216 (1965).Google Scholar
14. Ilong, M., Fleming, R.M., Kwo, J., Schneemeyer, L.F., Waszczak, I.V., Mannaerts, I.P., Majkrzak, C.F., Gibbs, D.B., and Bohr, J., J. Appl. Phys. 61, 4052 (1987).Google Scholar