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The Search for Interstitial Dislocation Loops Produced in Displacement Cascades at 20K in Copper

Published online by Cambridge University Press:  15 February 2011

M. A. Kirk
Affiliation:
Materials Science Division, Argonne National Laboratory, Argonne, Illinois 60439, USA
M. L. Jenkins
Affiliation:
Department of Materials, University of Oxford, Parks Rd., Oxford OX1 3PH, UK
H. Fukushima
Affiliation:
Faculty of Engineering, Hiroshima University, Higashi-Hiroshima 739-8527, Japan
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Abstract

A low-temperature in situ ion-irradiation and annealing experiment has been performed by TEM in copper. Most defect clusters which persisted through an anneal to 120 K showed no size changes within the resolution (0.5 nm) of a new weak-beam sizing technique. Of 55 defects measured under a range of weakly diffracting conditions, 7 showed measurable size decreases while 3 showed size increases. We argue that these clusters are likely to be of vacancy and interstitial nature, respectively. Also on annealing to 120 K a fraction of about 25% of the clusters formed by irradiation with 600 kV Cu+ ions at 20 K disappeared, while a similar number of clusters appeared in different locations.

Type
Research Article
Copyright
Copyright © Materials Research Society 1999

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References

[1] Rubia, T. D. de la and Guinan, M. W., Phys.Rev.Lett. 66, 2766 (1991).Google Scholar
[2] Foreman, A. J. E., Phythian, W. J. and English, C. A., Phil.Mag. A 66, 671 (1992).Google Scholar
[3] Bacon, D. J., Calder, A. F., Gao, F., Kapinos, V. G. and Wooding, S. J., Nucl. Inst. Meth. B 102, 51 (1995).Google Scholar
[4] Fukushima, H., Shimomura, Y. and Guinan, M. W., J. Nucl. Mat. 155–157, 1205 (1988).Google Scholar
[5] Ruault, M. O., Bemas, H. and Chaumont, J., Phil. Mag. A 39, 757 (1979).Google Scholar
[6] Fukushima, H., Jenkins, M. L. and Kirk, M. A., Phil. Mag. A 75, 1567 (1997).Google Scholar
[7] Fukushima, H., Jenkins, M. L. and Kirk, M. A., Phil. Mag. A 75, 1583 (1997).Google Scholar
[8] Frischherz, M. C., Kirk, M. A., Zhang, J. P., and Weber, H. W., Phil. Mag. A 67. 1347 (1993).Google Scholar
[9] Ziegler, J. F., Biersack, J. P., and Littmark, U., The Stopping and Range of Ions in Solids, Pergamon, NY, 1985.Google Scholar
[10] Jenkins, M. L., Kirk, M. A. and Fukushima, H., submitted to J. Electron MicroscopyGoogle Scholar
[11] Vetrano, J. S., Robertson, I. M., and Kirk, M. A., Scripta Met. 24, 157 (1990).Google Scholar