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Preparation of Multicomponent Ceramic Powders by Sol-Gel Processing

Published online by Cambridge University Press:  28 February 2011

J.R. Bartlett
Affiliation:
Advanced Materials Program,Australian Nuclear Science and Technology Organisation,Private Mail Bag No. 1,Menai,N.S.W. 2234.Australia.
J.L. Woolfrey
Affiliation:
Advanced Materials Program,Australian Nuclear Science and Technology Organisation,Private Mail Bag No. 1,Menai,N.S.W. 2234.Australia.
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Abstract

Sol-gel methods have been applied to the production of the multicomponent ceramic, Synroc B. These techniques involved the hydrolysis of a mixture of Ti and Zr, alkoxides peptising to form a sol and subsequent sorption of Al3+, Ba2+ and Ca2+ cations under acidic conditions. Powder properties were examined by a variety of techniques, including electron microscopy, x-ray diffraction, N2 sorption, and differential thermal analysis. The effects of processing conditions on the physical properties of the powders are discussed.

Type
Research Article
Copyright
Copyright © Materials Research Society 1990

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References

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