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Preparation of Free-Standing PZT and Gold Nanoparticles

Published online by Cambridge University Press:  15 February 2011

R. N. Das
R. N. Das*
Affiliation:
Cornell University, Materials Science and Engineering, Ithaca, NY-14850 Department of Chemistry, Indian Institute of Technology, Kharagpur, West Bengal 721302, India
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Abstract

Free-standing PZT (Lead Zirconate Titanate ) and Gold nanoparticles (ceramic and metal) have been prepared by complex process. In case of PZT, the process involves the preparation of metal ion complex (ligand) solution followed by evaporation. Complete evaporation results in fluffy dried mass. Calcination of dried mass at low temperature produces free-standing PZT nanoparticles. The concept of the process involves choice of correct metal ion complex, stoiochiometry and drying conditions to produce free-standing individual nanoparticles. Similar process has been used to prepare free-standing gold nanoparticles where individual gold form complex with the ligands (complexing agents) to produce free-standing nanoparticles.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 879: Symposium Z – Chemistry of Nanomaterial Synthesis and Processing , 2005 , Z10.19
Copyright
Copyright © Materials Research Society 2005

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References

1. Banerjee, A. and Bose, S., Chem. Mater. 16, 5610 (2004)Google Scholar
2. Campbell, S.A., Kortshagen, U., Bapat, A., Dong, Y., Hilchie, S., Shen, Z., JOM 56, 26 (2004)Google Scholar
3. Viswanatha, R., Sapra, S., Gupta, S. Sen, Satpati, B., Satyam, PV, Dev, BN, Sarma, DD J. Phys Chem B 108, 6303(2004).Google Scholar
4. Xu, R., Zeng, HC, J. Phys Chem B 107, 926(2003)Google Scholar
5. Liu, C., Zou, BS, Rondinone, AJ, Zhang, ZJ J Am Chem Soc., 123, 4344 (2001)Google Scholar
6. Das, R. N., Pathak, A., Pramanik, P., J Am Ceram Soc., 81, 3357(1998)Google Scholar
7. Shannigrahi, S. R., Choudhary, R.N.P., Acharya, H. N., J. Appl. Phys., 85, 1713(1999)Google Scholar
8. Chen, S., Langmuir 15, 7551(1999)Google Scholar
9. Das, R. N., Bose, S. and Bandyopadhya, A, “Nanocrystalline a-Al2O3fromsucrose” J. Am. Ceram. Soc. 84, 2421(2001)Google Scholar