Hostname: page-component-78c5997874-g7gxr Total loading time: 0 Render date: 2024-11-19T23:54:29.332Z Has data issue: false hasContentIssue false

Plastic and Elastic Behavior of Sputtered Bilayered Films by Nanoindedtation

Published online by Cambridge University Press:  10 February 2011

N. Kikuchi
Affiliation:
Advanced Materials Science R& D Center, Kanazawa Institute of Technology, 3-1 Yatsukaho, Matto, Kanazawa 924-0838JAPAN
E. Kusano
Affiliation:
Advanced Materials Science R& D Center, Kanazawa Institute of Technology, 3-1 Yatsukaho, Matto, Kanazawa 924-0838JAPAN
Y. Sawahira
Affiliation:
Advanced Materials Science R& D Center, Kanazawa Institute of Technology, 3-1 Yatsukaho, Matto, Kanazawa 924-0838JAPAN
A. Kinbara
Affiliation:
Advanced Materials Science R& D Center, Kanazawa Institute of Technology, 3-1 Yatsukaho, Matto, Kanazawa 924-0838JAPAN
Get access

Abstract

Deformation behavior of sputtered Al/TiN and Cu/TiN bilayered films was examined by using dissipated and elastic energies estimated from the area enclosed by the load-displacement curve of nanoindentation. These films studied consisted of TiN top-layer of 500 nm and Al or Cu underlayer of 0 - 500 nm on glass or sapphire substrate. The dissipated energy for plastic deformation increased with increasing thickness of metal underlayer, while the elastic energy remained constant. A decrease in plastic energy was observed by changing the underlayer material from Al to Cu. Further, a reduction in elastic energy was observed when a sapphire was used as a substrate. Experimental results show that the plastic deformation mainly occurred in metal underlayer and the elastic deformation did in TiN layer and in the substrate. It was concluded that the yield stress and elastic modulus of layers and substrate strongly affect the deformation behavior of the films.

Type
Research Article
Copyright
Copyright © Materials Research Society 2000

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

[1] Pharr, G.M. and Oliver, W.C., MRS Bulletin 17, 28 (1992).Google Scholar
[2] Febes, B.D., Oliver, W.C., McKee, R.A. and Walker, F.J., J. Mater. Res. 7, 3056 (1992)Google Scholar
[3] Wang, H. F., Bell, T. and Zheng, S., Thin Solid Films 258, 198 (1995).Google Scholar
[4] Cai, X. and Bangert, H., Thin Solid Films 264, 59 (1995).Google Scholar
[5] Lichinchi, M., Lenardi, C., Haupt, J. and Vitali, R., Thin Solid Films 312, 240 (1998).Google Scholar
[6] Doerner, M.F., Gardner, D.S. and Nix, W.D., J. Mater. Res. 1, 945 (1987).Google Scholar
[7] Kusano, E., Kitagawa, M., Nanto, H. and Kinbara, A.: J. Vac. Sci. Technol. A 16, 1272 (1998).Google Scholar
[8] Kusano, E., Kitagawa, M., Nanto, H. and Kinbara, A. in Thin Films; Stress and Mechanical Properties, edited by Cammarata, R.C., Busso, E.P., Nastasi, M., and Oliver, W.C. (Mater. Res. Soc. Proc. 505, Warrendale, PA, 1998) pp. 577582.Google Scholar
[9] Kikuchi, N., Kitagawa, M., Sato, A., Kusano, E., Nanto, H. and Kinbara, A., Surf. Coat. Tech. to be published.Google Scholar
[10] Sawahira, Y., Satoh, A., Kikuchi, N., Kusano, E., Nanto, H. and Kinbara, A., J. Vac. Soc. Jpn. 42,652 (1999).Google Scholar
[11] The Japan Institute of Metals Ed., Data Book of Metals, (Maruzen publications, Japan, 1993), p.31.Google Scholar