Hostname: page-component-cd9895bd7-q99xh Total loading time: 0 Render date: 2024-12-27T02:31:23.959Z Has data issue: false hasContentIssue false

New Perspectives in Monitoring the Flame Synthesis of Iron Oxide Nanoparticles: Addressing Solid and Gas-Phase Diagnostics Challenges

Published online by Cambridge University Press:  08 April 2015

Igor Rahinov*
Affiliation:
Department of Natural Sciences, The Open University of Israel, Raanana 4353701, Israel.
Marina Poliak
Affiliation:
School of Chemistry, Tel Aviv University, Tel Aviv 69978, Israel.
Alexey Fomin
Affiliation:
School of Chemistry, Tel Aviv University, Tel Aviv 69978, Israel.
Vladimir Tsionsky
Affiliation:
School of Chemistry, Tel Aviv University, Tel Aviv 69978, Israel.
Sergey Cheskis
Affiliation:
School of Chemistry, Tel Aviv University, Tel Aviv 69978, Israel.
*
Get access

Abstract

Several techniques for in-situ monitoring and characterization of flame synthesized nanoparticles are described with the goal of gaining further insight into the mechanisms governing nanoparticle (NP) formation in flame reactors. These include: a combined particle mass spectrometer - quartz crystal microbalance apparatus (PMS-QCM); The Light Induced Detuning –Quartz Crystal Microbalance (LID-QCM) method; Application of Intra Cavity Laser Absorption Spectroscopy (ICLAS) for monitoring gas phase intermediates in a particle laden environment.

Type
Articles
Copyright
Copyright © Materials Research Society 2015 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

Strobel, R., Pratsinis, S.E., J.Mater.Chem. 17, 47434756 (2007)CrossRefGoogle Scholar
Mishra, Y.K., Kaps, S. et al. . Part. Part. Syst. Charact, 30, 775783 (2013)CrossRefGoogle Scholar
Lu, H., Salabas, E.L., Schüth, F., Angew. Chem. (Int. ed.) 46, 12221244 (2007)CrossRefGoogle Scholar
Janzen, C., Roth, P., Combust. Flame 125, 11501161 (2001)CrossRefGoogle Scholar
Fomin, A., Poliak, M., Rahinov, I., Tsionsky, V. and Cheskis, S., Combust. Flame 160, 2131 – 214 (2013)CrossRefGoogle Scholar
Fomin, A., Poliak, M., Tsionsky, V., Cheskis, S., Rahinov, I., Sensors and Actuators B 202, 861865 (2014)CrossRefGoogle Scholar
Goldman, A., Cheskis, S., Appl. Phys. B Lasers Opt. 92(2), 281 (2008)CrossRefGoogle Scholar
Rahinov, I., Fomin, A., Poliak, M., Cheskis, S., Appl. Phys. B, 117(1), 317323 (2014)CrossRefGoogle Scholar
Poliak, M., Fomin, A., Tsionsky, V., Cheskis, S., Wlokas, I. and Rahinov, I. Phys. Chem. Chem. Phys., 17, 680685 (2015)CrossRefGoogle Scholar
Wlokas, I., Faccinetto, A., Tribalet, B., Schulz, C. and Kempf, A., Int. J. Chem. Kinet.,45, 487498 (2013)CrossRefGoogle Scholar