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Interphase Study By Xps of Sol-Gel ZrO2 Coatings On Stainless Steel

Published online by Cambridge University Press:  21 February 2011

Jean-Francois Quinson ,
Chantal Chino ,
Anne-Marie De Becdelievre  and
Christian Guizard
Jean-Francois Quinson
Affiliation:
Département de Chimie Appliquée, CNRS ERS 69, UCB-Lyon 1,43 Bd du 11 Novembre 1918, 69622 VILLEURBANNE Cedex, FRANCE
Chantal Chino
Affiliation:
Département de Chimie Appliquée, CNRS ERS 69, UCB-Lyon 1,43 Bd du 11 Novembre 1918, 69622 VILLEURBANNE Cedex, FRANCE
Anne-Marie De Becdelievre
Affiliation:
Département de Chimie Appliquée, CNRS ERS 69, UCB-Lyon 1,43 Bd du 11 Novembre 1918, 69622 VILLEURBANNE Cedex, FRANCE
Christian Guizard
Affiliation:
Laboratoire des Matériaux et Procédés Membranaires, CNRS EP 50, ENSC, 8 rue de l'Ecole Normale, 34053 MONTPELLIER Cedex 1, FRANCE
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Abstract

ZrO2 coatings were obtained by the the alkoxide route and deposited onto stainless steel using the dip coating technique. The starting solutions were prepared by mixing zirconium tetrabutoxide, isopropanol, acetylacetone. The water content for the hydrolitic reaction arose from the atmosphere moisture.

Useful information for the structural organization of the zirconia/steel interphase is given by XPS analysis.

It is found that during firing treatment, the main components (Fe, Cr, Ni) of the stainless steel diffuse into the ceramic coating. XPS data allow to describe the chemical composition variation from the bulk substrate to the outer coating surface.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 346: Symposium N – Better Ceramics Through Chemistry VI , 1994 , 703
Copyright
Copyright © Materials Research Society 1998

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References

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