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High Sensitivity Convergent Beam Electron Diffraction for the Determination of the Tetragonal Distortion of Epitaxial Films

Published online by Cambridge University Press:  10 February 2011

C. Schuer
Affiliation:
now at: Infineon Technologies AG, A-9500 Villach (Austria)
M. Leicht
Affiliation:
Institute for Microcharacterisation, Friedrich-Alexander-University Erlangen-Nuremberg, Cauerstr. 6, D-91058 Erlangen (Germany), [email protected]
T. Marek
Affiliation:
now at: Infineon Technologies AG, A-9500 Villach (Austria)
H.P. Strunk
Affiliation:
now at: Infineon Technologies AG, A-9500 Villach (Austria)
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Abstract

We have optimized the sensitivity of convergent beam electron diffraction (CBED) by orienting the specimen such that the central (000) diffraction disc shows a pattern of defect lines that are most sensitive to tetragonal distortion. We compare the position of these lines in the experimentally obtained patterns with results from computer simulations, which need to be based on dynamical diffraction theory. In both experimental and simulated patterns the positions of the defect lines are determined by applying a Hough transformation. As a result of this optimized approach, we can measure the tetragonal distortion of a low temperature grown GaAs layer as low as 0.04%.

Type
Research Article
Copyright
Copyright © Materials Research Society 2001

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