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Growth Morphology of InN Thin Films by Scanning Tunneling and Atomic Force Microscopies and X-Ray Scattering

Published online by Cambridge University Press:  15 February 2011

Wayne A. Bryden
Affiliation:
Applied Physics Laboratory, The Johns Hopkins University, Laurel, MD 20723
Marilyn E. Hawley
Affiliation:
Los Alamos National Laboratory, Los Alamos, NM 87545
Scott A. Ecelberger
Affiliation:
Applied Physics Laboratory, The Johns Hopkins University, Laurel, MD 20723
Thomas J. Kistenmacher
Affiliation:
Applied Physics Laboratory, The Johns Hopkins University, Laurel, MD 20723
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The evolution of the growth morphology of thin films of InN on (00.1) sapphire and on (00.1) sapphire prenudeated by a layer of AIN have been followed as a function of the thickness of the InN overlayer. The InN thin films and the AIN nucleation layers were deposited by reactive magnetron sputtering and first characterized by X-ray scattering, profilometry, and electrical transport. These AIN-nucleated InN films displayed heteroepitaxial grains, and high Hall mobility -even in the limit of InN overlayer on the order of 20-40Å. In parallel, InN films of varying thickness were grown directly onto (00.1) sapphire. These films showed a mixture of textured and heteroepitaxial grains, and lower Hall mobility. Atomic force and scanning tunneling microscopy studies have focussed on the morphology of the InN films with thicknesses: (a) much smaller than the AIN nucleation layer; and, (b) near the morphological transition that occurs at ∼1μm and has been attributed to the crossover from a 2D to a 3D growth mechanism. Additional correlations of X-ray structural coherence with growth mode are also examined.

Type
Research Article
Copyright
Copyright © Materials Research Society 1993

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References

1 For recent reviews see J. I. Pankove in Diamond, Boron Nitride, Silicon Carbide and Related Wide Bandgap Semiconductors, edited by Glass, J. T., Messier, R. F., and Fujimori, N. (Mater. Res. Soc. Proc. 162, Pittsburgh, PA, 1990) pp.515522; R. F. Davis in The Physics and Chemistry of Carbides, Nitrides and Borides, edited by R. Freer (Kluwer, Amsterdam, 1990) pp. 653–669; T.Matsuoka, J. Cryst. Growth 124, 433 (1992).Google Scholar
2. See, for example, Bauer, E. G. et al., J. Mater. Res. 5, 852 (1990); R. Kern, G.Le Lay, and J. J. Metois, in Current Topics in Materials Science, edited by E. Kaldis (North-Holland, Amsterdam, 1979), p. 130.Google Scholar
3. Amano, H., Sawaki, N., Akasaki, I., and Toyoda, Y., Appl. Phys. Lett. 48, 415 (1988); H.Amano, I.Akasaki, K.Hiramatsu, N.Koide and N.Sawaki,Thin Solid Films 163, 415 (1988); D. K.Wickenden, T. J.Kistenmacher, W. A.Bryden, J. S. Morgan and A. Estes Wickenden in Heteroepitaxy of Dissimilar Materials, edited by R. F. C.Farrow, J. P.Harbison, P. S. Peercy and A. Zangwill (Mater. Res. Soc. Proc. 221, Pittsburgh, PA, 1991) pp. 167–172; M.Asif Kahn, J. M.Van Hove, J. N.Kuznia, and D. T.Olson, Appl. Phys. Lett. 58, 2408 (1991).Google Scholar
4. Choi, C.–H., Hultman, L., Choi, W.–A., and Barnett, S. A., J. Vac. Sci. Technol. B 9, 221 (1991).Google Scholar
5. Kistenmacher, T. J., Bryden, W. A., Morgan, J. S. and Poehler, T. O.,. j.Appl. Phys. 68, 1541 (1990); W. A.Bryden, J. S.Morgan, R.Fainchtein and T. J. Kistenmacher, Thin Solid Films 213, 86 (1992).Google Scholar
6. Kistenmacher, T. J. and Bryden, W. A., Appl. Phys. Lett. 59, 1844 (1991).Google Scholar
7. Bryden, W. A., Morgan, J. S., Kistenmacher, T. J., Dayan, D., Fainchtein, R. and Poehler, T.O., in Diamond, Boron Nitride, Silicon Carbide and Related Wide Bandgap Semiconductors, edited by J. T.Glass, R. F.Messier, and N. Fujimori (Mater. Res. Soc. Proc. 162, Pittsburgh, PA, 1990) pp.567572.Google Scholar