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Published online by Cambridge University Press: 28 February 2011
Annealing and quenching experiments in a thermogravimetric analysis apparatus are used to vary the oxygen content in La2Ni1‐yCuy04+δ, followed by magnetic susceptibility and x‐ray diffraction experiments. These studies show that for certain δ, transition to antiferromagnetism occurs with TN < 20 K. The effect of Cu doping (y = 0.01 and 0.05) on TN is negligible.