Hostname: page-component-586b7cd67f-tf8b9 Total loading time: 0 Render date: 2024-11-25T17:52:36.324Z Has data issue: false hasContentIssue false

Determination Of Temperature Dependent Unstressed Lattice Spacings In Crystalline Thin Films On Substrates

Published online by Cambridge University Press:  10 February 2011

G. Cornella
Affiliation:
Department of Materials Science and Engineering, Stanford University, Stanford, CA 94305-2205
S. Lee
Affiliation:
Department of Materials Science and Engineering, Stanford University, Stanford, CA 94305-2205
O. Kraft
Affiliation:
Department of Materials Science and Engineering, Stanford University, Stanford, CA 94305-2205
W. D. Nix
Affiliation:
Department of Materials Science and Engineering, Stanford University, Stanford, CA 94305-2205
J. C. Bravman
Affiliation:
Department of Materials Science and Engineering, Stanford University, Stanford, CA 94305-2205
Get access

Abstract

X-ray strain analysis via Generalized Focusing Diffractometry (GFD) [1], and the concurrent need for accurate values of the unstrained lattice parameter, are discussed. A new method for determining the unstrained lattice parameter without knowledge of the elastic constants of the sample material is described. Stress measurements at varying temperatures, and extraction of the coefficient of thermal expansion from these measurements, are demonstrated for aluminum and gold films.

Type
Research Article
Copyright
Copyright © Materials Research Society 1998

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1.Flinn, P. A. and Waychunas, G. A., J. Vac. Sci. Technol. B 6, 1749 (1988).Google Scholar
2.Clemens, B. M. and Bain, J. A., Mater. Res. Bull. 17, 46 (1992).Google Scholar
3.Flinn, P. A., Gardner, D. S., and Nix, W. D., IEEE Trans. Electron Devices, Vol ED-34, 3, 689 (1987).Google Scholar
4.Flinn, P. A., in Thin Films: Stresses and Mechanical Properties, edited by Bravman, J. C., Nix, W. D., Barnett, D. M., and Smith, D. A. (Materials Research Society, Pittsburgh, PA, 1989), Vol.130, pp. 4151.Google Scholar
5.Besser, P. R., X-ray determination of thermal strains and stresses in thin aluminum films and lines, Ph.D. thesis 1993, Stanford University.Google Scholar
6.Zielinski, E. M., Vinci, R. P., and Bravman, J. C., J. Appl. Phys. 76, 4516 (1994).Google Scholar
7.Pearson, W. B., A Handbook of Lattice Spacings and Structures of Metals and Alloys (Pergamon Press, New York, 1958), p. 40.Google Scholar
8.Hosford, W. F., The Mechanics of Crystals and Textured Polycrystals (Oxford University Press, New York, Oxford, 1993), p. 16.Google Scholar
9.Harrison, R. D., Datenbuch Chemie, Physik. Vieweg Studium (Vieweg 1982).Google Scholar
10.Simmons, R. O. and Balluffi, R. W., Phys. Rev. 117, 52 (1960).Google Scholar