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Correlation of Silver Size Nanoparticles Between TEM and QELS

Published online by Cambridge University Press:  01 February 2011

A. Ruíz-Baltazar ,
A. Escobedo ,
U. Pal ,
R. Pérez  and
G. Rosas
A. Ruíz-Baltazar
Affiliation:
Instituto de Investigaciones Metalúrgicas, UMSNH, Edificio U, Ciudad Universitaria, CP 58060, Morelia Michoacán, MEXICO, Email: [email protected]
A. Escobedo
Affiliation:
Instituto de Física, BUAP, Edif. 14, Ciudad Universitaria, C.P. 72570, Puebla, Puebla, MÉXICO
U. Pal
Affiliation:
Instituto de Física, BUAP, Edif. 14, Ciudad Universitaria, C.P. 72570, Puebla, Puebla, MÉXICO
R. Pérez
Affiliation:
Instituto de Ciencias Físicas, Universidad Nacional Autónoma de México, P.O. Box 48–3, Cuernavaca, Morelos, 62251, MEXICO
G. Rosas
Affiliation:
Instituto de Investigaciones Metalúrgicas, UMSNH, Edificio U, Ciudad Universitaria, CP 58060, Morelia Michoacán, MEXICO, Email: [email protected]
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Abstract

In this work, silver nanoparticles were synthesized by two methods: polyol and chemical reduction using sodium borohydride (NaBH4). In both cases, silver nitrate was employed as starting metallic salt and Poly-vinyl pyrrolidone (PVP) as surfactant agent. The average nanoparticles size was correlated by transmission electron microscopy (TEM) and quasielastic light scattering (QELS). The experimental results indicate that the average particle sizes measured by QELS were slightly higher than those obtained directly by TEM. Therefore, this work confirms that the QELS technique can give rapid and approximate average-particle size values in comparison with those obtained through TEM direct observations.

Keywords

Agchemical synthesistransmission electron microscopy (TEM)nanoscalenanostructure
Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 1275: Structural and Chemical Characterization of Metals, Alloys and Compounds , 2010 , S3-P102
Copyright
Copyright © Materials Research Society 2010

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