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Exploration of Processing Parameters of Vacuum Assisted Micelle Confinement Synthesis of Spherical CL-20 Microparticles

Published online by Cambridge University Press:  02 January 2018

Kaifu Bian ,
Leanne Alarid ,
David Rosenberg  and
Hongyou Fan
Kaifu Bian
Affiliation:
Sandia National Laboratories, Albuquerque, New Mexico 87185, U.S.A.
Leanne Alarid
Affiliation:
Sandia National Laboratories, Albuquerque, New Mexico 87185, U.S.A.
David Rosenberg
Affiliation:
Sandia National Laboratories, Albuquerque, New Mexico 87185, U.S.A.
Hongyou Fan*
Affiliation:
Sandia National Laboratories, Albuquerque, New Mexico 87185, U.S.A. Department of Chemical and Biological Engineering, Center for Micro-Engineered Materials, University of New Mexico, Albuquerque, New Mexico 87123, U.S.A.
*
*(Email: [email protected])
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Abstract

We recently developed a vacuum assisted micelle confinement synthesis for spherical microparticles of CL-20 with outstanding monodispersity. These microparticles are promising energetic material for explosive devices with enhanced and predictable performances. In this work, to facilitate further development and application of this synthesis, the particle growth process was monitored by in-situ dynamic light scattering measurements. The result was interpreted by a finite element model to obtain critical parameters. These parameters were then used to predict the behavior and product quality of batch synthesis under various operation conditions.

Keywords

colloidnanoscalesimulation
Type
Articles
Information
MRS Advances , Volume 3 , Issue 11: Theory, Characterization and Modeling , 2018 , pp. 553 - 561
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Copyright
Copyright © Materials Research Society 2017 

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References

REFERENCES

Ghosh, M., Venkatesan, V., Mandave, S., Banerjee, S., Sikder, N., Sikder, A.K. and Bhattacharya, B.: Crystal Growth and Design 14, 5053 (2014).Google Scholar
Nielsen, A.T., Nissan, R.A., Vanderah, D.J., Coon, C.L., Gilardi, R.D., George, C.F. and Flippen-Anderson, J.: J. Org. Chem. 55, 1459 (1990).CrossRefGoogle Scholar
Nair, U.R., Sivabalan, R., Gore, G.M., Geetha, M., Asthana, S.N. and Singh, H.: Combust. Explos. and Shock Waves 41, 121 (2005).Google Scholar
Talawar, M.B., Sivabalan, R., Anniyappan, M., Gore, G.M., Asthana, S.N. and Gandhe, B.R.: Combust. Explos. and Shock Waves 43, 62 (2007).Google Scholar
Liu, K., Zhang, G., Luan, J., Chen, Z., Su, P. and Shu, Y.: J. Mol. Struct. 1110, 91 (2016).Google Scholar
Simpson, R.L., Urtiew, P.A., Ornellas, D.L., Moody, G.L., Scribner, K.J. and Hoffman, D.M.: Propellants, Explos., and Pyrotech. 22, 249 (1997).Google Scholar
Bayat, Y., Zarandi, M., Zarei, M.A., Soleyman, R. and Zeynali, V.: J. Mol. Liquids 193, 83 (2014).CrossRefGoogle Scholar
Xu, J., Tian, Y., Liu, Y., Zhang, H., Shu, Y. and Sun, J.: J. Crst. Growth 354, 13 (2012).Google Scholar
Yang, Z., Zeng, Q., Zhou, X., Zhang, Q., Nie, F., Huang, H. and Li, H.: RSC Adv. 4, 65121 (2014).Google Scholar
Urbelis, J.H. and Swift, J.A.: Cryst. Growth Des. 14, 1642 (2014).CrossRefGoogle Scholar
Bian, K., Alarid, L., Rosenberg, D. and Fan, H.: unpublished.Google Scholar
Tyn, M.T. and Calus, W.F.: Diffusion Coefficients in Dilute Binary Liquid Mixtures. J. Chem. Eng. Data 20 (1975).Google Scholar
Gavira, J.A.: Current Trends in Protein Crystallization. Archives of Biochemistry and Biophysics 602, 3 (2016).Google Scholar
Ghosh, M., Banerjee, S., Khan, M., Sikder, N. and Sikder, A.: Phys. Chem. Chem. Phys. 18, 23554 (2016).CrossRefGoogle Scholar