Hostname: page-component-586b7cd67f-rdxmf Total loading time: 0 Render date: 2024-11-26T17:27:16.188Z Has data issue: false hasContentIssue false
  • English
  • Français

Statistical student's t-test in carbon nanospheres synthesis from cis-1,4-polyisoprene

Published online by Cambridge University Press:  28 October 2020

Jaime A. Guzmán-Fuentes Open the ORCID record for Jaime A. Guzmán-Fuentes [Opens in a new window] ,
José J. Contreras-Navarrete ,
Erasmo Cadenas-Calderón ,
Jael M. Ambriz-Torres ,
Diana L. García-Ruíz ,
Carmen J. Gutiérrez-García ,
Francisco G. Granados-Martínez ,
Leandro García-González ,
Luis Zamora-Peredo  and
Yesenia Arredondo-León
...Show all authors
Jaime A. Guzmán-Fuentes
Affiliation:
Universidad Michoacana de San Nicolás de Hidalgo, Facultad de Ingeniería Mecánica, México.
José J. Contreras-Navarrete
Affiliation:
Tecnológico Nacional de México/Instituto Tecnológico de Morelia, División de Estudios de Posgrado e Investigación, México.
Erasmo Cadenas-Calderón
Affiliation:
Universidad Michoacana de San Nicolás de Hidalgo, Facultad de Ingeniería Mecánica, México.
Jael M. Ambriz-Torres
Affiliation:
Tecnológico Nacional de México/Instituto Tecnológico de Morelia, División de Estudios de Posgrado e Investigación, México.
Diana L. García-Ruíz
Affiliation:
Universidad Michoacana de San Nicolás de Hidalgo, Facultad de Ingeniería Mecánica, México.
Carmen J. Gutiérrez-García
Affiliation:
Universidad Michoacana de San Nicolás de Hidalgo, Facultad de Ingeniería Mecánica, México.
Francisco G. Granados-Martínez
Affiliation:
Instituto de Investigaciones en Materiales, Universidad Nacional Autónoma de México, Campus Morelia, México.
Leandro García-González
Affiliation:
Centro de Investigación en Micro y Nanotecnología, Universidad Veracruzana, México.
Luis Zamora-Peredo
Affiliation:
Centro de Investigación en Micro y Nanotecnología, Universidad Veracruzana, México.
Yesenia Arredondo-León
Affiliation:
Escuela Nacional de Estudios Superiores, Universidad Nacional Autónoma de México, Campus Morelia, México.
Orlando Hernandez-Cristobal
Affiliation:
Escuela Nacional de Estudios Superiores, Universidad Nacional Autónoma de México, Campus Morelia, México.
Lada Domratcheva-Lvova*
Affiliation:
Universidad Michoacana de San Nicolás de Hidalgo, Facultad de Ingeniería Mecánica, México.
*
[email protected]
Get access

Abstract

A student's t-test was applied in carbon nanospheres synthesis from cis-1,4-polyisoprene considering the green chemical principles. The synthesis was carried out by Chemical Vapor Deposition method with a quartz tube reactor using an AISI 304 steel bar as catalyst. It was possible to obtain two types of different samples, one from the surface of the steel bar (catalyst) and another from the quartz tube surface (without catalyst) in the same experiment. Carbon spheres were observed in both samples by micrographs obtained by FESEM. The Raman and FTIR spectroscopies shown characteristic bands of this carbon structures (G and D). The results obtained by student's t-test proved a statistical significance between spheres means of samples collected from steel bar and quartz tube surface.

Type
Articles
Information
MRS Advances , Volume 5 , Issue 63: International Materials Research Congress XXIX , 2020 , pp. 3371 - 3377
Check for updates
Copyright
Copyright © The Author(s), 2020, published on behalf of Materials Research Society by Cambridge University Press

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Kumar, M., Ando, Y., Diamond Relat. Mater. 12(10-11), 1845, (2003).CrossRefGoogle Scholar
Ghosh, P., Soga, T., Afre, R. A., Jimbo, T., Alloy, J.. Compd. 462(1), 289, (2008).CrossRefGoogle Scholar
Ghosh, P., Afre, R.A., Soga, T., Jimbo, T., Mat. Lett. 61(17), 3768, (2007).CrossRefGoogle Scholar
Paul, S., Samdarshi, S. K., New Carbon Mater. 26(2), 85-88, (2011).CrossRefGoogle Scholar
Ambriz-Torres, J. M., Gutiérrez-García, C. J., García-Ruiz, D. L., Contreras-Navarrete, J. J., Granados-Martínez, F. G., Flores-Ramírez, N., Mondragón-Sánchez, M. L., García-González, L., Zamora-Peredo, L., Hernández-Cristóbal, O., Méndez, F., Domratcheva-Lvova, L.. J. Mater. Sci: Mater. Electron. 31, 7411 (2020).Google Scholar
Thostenson, E. T., Chou, Tsu-Wei, J. Phys. D: Appl. Phys. 36, 573, (2003).CrossRefGoogle Scholar
Granados-Martínez, F. G., Contreras-Navarrete, J. J., Ambriz-Torres, J. M., Gutiérrez-García, C. J., García-Ruiz, D. L., Guzmán-Fuentes, J. A., Flores-Ramírez, N., Cisneros-Magaña, M. R., García-González, L., Zamora-Peredo, L., Domratcheva-Lvova, L., MRS Advances 3(63), 3757, (2018).CrossRefGoogle Scholar
Islam, M. S., Deng, Y., Tong, L., Faisal, S. N., Roy, A. K., Minett, A. I., Gomes, V. G., Carbon 96, 701, (2016).10.1016/j.carbon.2015.10.002CrossRefGoogle Scholar
Lucas Flores, O., Kharissova, O. V., Ortiz Méndez, U., Leija Gutiérrez, H., de Casas Ortiz, E., Kharisov, B. I., J. Chem., (2013).Google Scholar
Li, Jing, Lu, Yijiang, Meyyappan, M., IEEE Sensors J. 6(5), 1047, (2006).CrossRefGoogle Scholar
Yadav, Manishkumar D., Dasgupta, Kinshuk, Patwardhan, Ashwin W., Joshi, Jyeshtharaj B., Ind. Eng. Chem. Res. 56(44), 12407, (2017).CrossRefGoogle Scholar
William, M. M., Terry, L. S., Statistics for engineering and the sciences. Sixth ed. (CRC Press, Taylor and Francis Group, New York, 2016).Google Scholar
de Marco, B. A., Rechelo, B. S., Tótoli, E. G., Kogawa, A. C., Nunes Salgado, H. R.. Saudi Pharm. J. 27(1), 1, (2019).CrossRefGoogle Scholar
Basiuk, E. V., Basiuk, V. A., J. Nanosci. Nanotechnol. 14, 644, (2014).CrossRefGoogle Scholar
Islam, M. R., Inter. J. Phys. & Math. 1(1), 37, (2018).Google Scholar
Deshmukh, A. A., Mhlanga, S. D., Coville, N. J.. Mater. Sci. Eng. R Rep. 70, 1, (2010).CrossRefGoogle Scholar
Gutiérrez García, C. J., Ambriz Torres, J. M., Contreras Navarrete, J. J., Granados Martínez, F. G., García Ruiz, D. L., …, Domratcheva Lvova, L., Phys. E: Low-dimens. Syst. and Nanostruct. 112, 78, (2019).CrossRefGoogle Scholar
Buchholz, D. B., Doherty, S. P., Chang, R. P. H., Carbon 41, 1625, (2003).CrossRefGoogle Scholar
Dresselhaus, M. S., Dresselhaus, G., Saito, R., Jorio, A., Phys. Rep. 409, 47, (2005).CrossRefGoogle Scholar
Brown, S. D. M., Jorio, A., Dresselhaus, M. S., Dresselhaus, G., Phys. Rev. B 64, 073403, (2001).CrossRefGoogle Scholar
Pérez Martínez, C. S., Ortíz del Toro, P. J., Espectroscopía: Introducción/UV-Visible/IR-Raman/Masas. (Editorial Félix Varela, La Habana, 2010) p. 171.Google Scholar
Ambriz-Torres, J. M., Gutiérrez-García, C. J., Contreras-Navarrete, J. J., Granados-Martínez, F. G., García-Ruiz, D. L., Flores-Ramírez, N., …, Domratcheva-Lvova, L., J. Elec. Materi. 48(8), 5161 (2019).CrossRefGoogle Scholar