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Quasi Crystal Al (1xxx)/Carbonised Coconut Shell Nanoparticles: Synthesis and Characterisation

Published online by Cambridge University Press:  17 April 2018

Sefiu A. Bello ,
Johnson O. Agunsoye ,
Jeleel A. Adebisi ,
Funsho O. Kolawole ,
Nasirudeen K. Raji  and
Suleiman B. Hassan
Sefiu A. Bello*
Affiliation:
Department of Materials Science and Engineering, Kwara State University, Malete, Nigeria Department of Metallurgical and Materials Engineering, University of Lagos, LagosNigeria
Johnson O. Agunsoye
Affiliation:
Department of Metallurgical and Materials Engineering, University of Lagos, LagosNigeria
Jeleel A. Adebisi
Affiliation:
Department of Metallurgical and Materials Engineering, University of Lagos, LagosNigeria Department of Metallurgical and Materials Engineering, University of Ilorin, IlorinNigeria
Funsho O. Kolawole
Affiliation:
Department of Metallurgical and Materials Engineering, University of Lagos, LagosNigeria Department of Metallurgical and Materials Engineering, Federal University of Oye-Ekiti, Nigeria
Nasirudeen K. Raji
Affiliation:
Department of Metallurgical Engineering, Yaba College of Technology, Lagos, Nigeria
Suleiman B. Hassan
Affiliation:
Department of Metallurgical and Materials Engineering, University of Lagos, LagosNigeria
*
*(Email: [email protected])
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Abstract

A novel synthesis of Al (1xxx)/carbonised coconut shell (CCS) nanoparticles using a ball milling technique was investigated. Initial Al/0.1%CCS powders of an average size of 51.06μm was milled for a period of 70 h. The milled particles at 16, 46 and 70 h were characterized using X-ray diffractomer (XRD), scanning electron microscope (SEM), transmission electron microscope and UV-Vis spectrophotometer. Result revealed that the calculated particle crystallite size from XRD aided with Scherrer’s equation is consistent with particle image sizes obtained from SEM aided with software. TEM image depicted variation in orientation and appearance of the Al 1xxx/0.1% CCS nanoparticles at different milling time. The wide variation in the particle size is attributable to different ball impacts on the individual powders during the ball milling process. Increased maximum absorbance observed with the milled particles when compared with the initial powders is an indication of quantum/nanosizing effect due to ball milling.

Keywords

Alcarbonizationcompositecompoundparticulate
Type
Articles
Information
MRS Advances , Volume 3 , Issue 42-43: African Materials Research Society 2017 , 2018 , pp. 2559 - 2571
Copyright
Copyright © Materials Research Society 2018 

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