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Water-based Si3N4 suspensions: Part I. Effect of processing routes on the surface chemistry and particle interactions

Published online by Cambridge University Press:  31 January 2011

C. Galassi ,
F. Bertoni ,
S. Ardizzone  and
C. L. Bianchi
C. Galassi
Affiliation:
IRTEC-CNR, Via Granarolo 64, I-48018 Faenza, Italy
F. Bertoni
Affiliation:
IRTEC-CNR, Via Granarolo 64, I-48018 Faenza, Italy
S. Ardizzone
Affiliation:
Department of Physical Chemistry and Electrochemistry, University of Milan, Via Golgi 19, I-20133 Milan, Italy
C. L. Bianchi
Affiliation:
Department of Physical Chemistry and Electrochemistry, University of Milan, Via Golgi 19, I-20133 Milan, Italy
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Extract

Si3N4 powders manufactured by two different preparative routes were characterized for the solid–liquid interfacial reactivity and surface composition. Three mixing processes were tried to investigate the modifications of silicon nitride particle surface in aqueous suspensions. The surfaces of the starting powders and the dried mixed powders were investigated by x-ray photoelectron spectroscopy to determine the nature and ratios of surface groups. Electroacoustic measurements show that no change occurs in the isoelectric point for the mixed Si3N4 powders while the milling/mixing process has a great influence on the zeta potential magnitude and particle size distribution.

Type
Articles
Information
Journal of Materials Research , Volume 15 , Issue 1 , January 2000 , pp. 155 - 163
Copyright
Copyright © Materials Research Society 2000

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