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Hydrothermal preparation of long nanowires of vanadium oxide

Published online by Cambridge University Press:  31 January 2011

Dengyu Pan ,
Zhang Shuyuan ,
Yiqing Chen  and
J. G. Hou
Dengyu Pan
Affiliation:
Structural Research Laboratory, University of Science and Technology of China, Hefei, Anhui 230026, People's Republic of China
Zhang Shuyuan
Affiliation:
Structural Research Laboratory, University of Science and Technology of China, Hefei, Anhui 230026, People's Republic of China
Yiqing Chen
Affiliation:
Structural Research Laboratory, University of Science and Technology of China, Hefei, Anhui 230026, People's Republic of China
J. G. Hou*
Affiliation:
Structural Research Laboratory, University of Science and Technology of China, Hefei, Anhui 230026, People's Republic of China
*
a)Address all correspondence to this author.[email protected]
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Abstract

Long beltlike nanowires were successfully synthesized for a semiconducting oxide of vanadium by a hydrothermal route at 180 °C for 5 h and were characterized by x-ray powder diffraction, energy dispersive -ray spectroscopy, and electron diffraction microscopy. The product is mainly layered V2O5 · 0.3H2O with a small fraction of V2O5 · xH2O (0.3 < x < 1.7) and V2O5 phases. The obtained nanowires, several tens of micrometers long and a few of tens of nanometers wide, are crystallized well, growing along the [010] direction. The effects of preparation conditions on the formation of the nanowires are discussed.

Type
Articles
Information
Journal of Materials Research , Volume 17 , Issue 8 , August 2002 , pp. 1981 - 1984
Copyright
Copyright © Materials Research Society 2002

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