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High-energy synchrotron x-ray techniques for studying irradiated materials

Published online by Cambridge University Press:  20 March 2015

Jun-Sang Park ,
Xuan Zhang ,
Hemant Sharma ,
Peter Kenesei ,
David Hoelzer ,
Meimei Li  and
Jonathan Almer
Jun-Sang Park
Affiliation:
Advanced Photon Source, Argonne National Laboratory, Lemont, Illinois 60439, USA
Xuan Zhang
Affiliation:
Nuclear Engineering Division, Argonne National Laboratory, Lemont, Illinois 60439, USA
Hemant Sharma
Affiliation:
Advanced Photon Source, Argonne National Laboratory, Lemont, Illinois 60439, USA
Peter Kenesei
Affiliation:
Advanced Photon Source, Argonne National Laboratory, Lemont, Illinois 60439, USA
David Hoelzer
Affiliation:
Materials Science and Technology Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831, USA
Meimei Li
Affiliation:
Nuclear Engineering Division, Argonne National Laboratory, Lemont, Illinois 60439, USA
Jonathan Almer*
Affiliation:
Advanced Photon Source, Argonne National Laboratory, Lemont, Illinois 60439, USA
*
a)Address all correspondence to this author. e-mail: [email protected]
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Abstract

High performance materials that can withstand radiation, heat, multiaxial stresses, and corrosive environment are necessary for the deployment of advanced nuclear energy systems. Nondestructive in situ experimental techniques utilizing high energy x-rays from synchrotron sources can be an attractive set of tools for engineers and scientists to investigate the structure–processing–property relationship systematically at smaller length scales and help build better material models. In this study, two unique and interconnected experimental techniques, namely, simultaneous small-angle/wide-angle x-ray scattering (SAXS/WAXS) and far-field high-energy diffraction microscopy (FF-HEDM) are presented. The changes in material state as Fe-based alloys are heated to high temperatures or subject to irradiation are examined using these techniques.

Keywords

x-ray diffraction (XRD)steelradiation effects
Type
Articles
Information
Journal of Materials Research , Volume 30 , Issue 9: Focus Issue: Characterization and Modeling of Radiation Damage on Materials: State of the Art, Challenges, and Protocols , 14 May 2015 , pp. 1380 - 1391
Copyright
Copyright © Materials Research Society 2015 

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Footnotes

Contributing Editor: Djamel Kaoumi

References

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