Hostname: page-component-586b7cd67f-rdxmf Total loading time: 0 Render date: 2024-11-23T07:36:26.212Z Has data issue: false hasContentIssue false

Fracture toughness in direct extruded Mg–Al–Zn alloys

Published online by Cambridge University Press:  31 January 2011

Hidetoshi Somekawa*
Affiliation:
Structural Metals Center, National Institute for Materials Science, Tsukuba, Ibaraki 305-0047, Japan
Han S. Kim
Affiliation:
Structural Metals Center, National Institute for Materials Science, Tsukuba, Ibaraki 305-0047, Japan
Alok Singh
Affiliation:
Structural Metals Center, National Institute for Materials Science, Tsukuba, Ibaraki 305-0047, Japan
Toshiji Mukai
Affiliation:
Structural Metals Center, National Institute for Materials Science, Tsukuba, Ibaraki 305-0047, Japan
*
a)Address all correspondence to this author. e-mail: [email protected]
Get access

Abstract

Fracture toughness and its deformed structures were investigated on a Mg–3Al–1Zn (AZ31) alloy processed by direct extrusion. The average grain sizes of the alloy after extrusion at temperatures of 473 and 573 K were 4.0 and 14.5 μm, respectively (i.e., fine-grained and coarse-grained alloys). The plane-strain fracture toughness, KIC, as determined by stretched zone analysis in fine-grained and coarse-grained alloys was estimated to be 24.9 and 22.7 MPam1/2, respectively. Microstructural observations of the fine-grained alloy after fracture toughness testing showed that non-basal slip and grain-boundary sliding was activated even at room temperature. In addition, the {10-12} deformation twins were observed despite the fine-grained structures. However, the fraction of deformation twins was reduced with grain refinement, which related to the enhancement of fracture toughness with grain refinement.

Type
Articles
Copyright
Copyright © Materials Research Society 2007

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1Somekawa, H.Mukai, T.: Effect of grain refinement on fracture toughness in extruded pure-magnesium. Scripta Mater. 53, 1059 2005CrossRefGoogle Scholar
2Barbagallo, S.Cerri, E.: Evaluation of the K IC and J IC fracture parameters in a sand AZ91 magnesium alloy. Eng. Fail. Anal. 11, 127 2004CrossRefGoogle Scholar
3Lee, S., Lee, S.H.Kim, D.H.: Effect of Y, Sr, and Nd additions on the microstructure mechanism of squeeze-cast AZ91-X magnesium alloys. Metall. Mater. Trans. A 29, 1221 1998CrossRefGoogle Scholar
4Purazrang, K., Kainer, K.U.Mordike, B.L.: Fracture toughness behavior of a magnesium alloy metal-matrix composite produced by the infiltration technique. Composites 22, 456 1991CrossRefGoogle Scholar
5Sasaki, T., Somekawa, H., Takara, A., Nishikawa, Y.Higashi, K.: Plane-strain fracture toughness on thin AZ31 wrought magnesium alloy sheets. Mater. Trans. 44, 986 2003CrossRefGoogle Scholar
6Somekawa, H.Mukai, T.: Fracture toughness in an extruded ZK60 magnesium alloy. Mater. Trans. 47, 995 2006CrossRefGoogle Scholar
7Somekawa, H., Singh, A.Mukai, T.: Effect of precipitate shapes on fracture toughness in extruded Mg-Zn-Zr magnesium alloys. J. Mater. Res. 22(4), 965 2007CrossRefGoogle Scholar
8Magnesium and magnesium alloys in ASM Specialty Handbook edited by M.M. Avedesian and H. Baker ASM International Materials Park, OH 1999 163Google Scholar
9Aluminum and aluminum alloys in ASM Specialty Handbook edited by J.R. Davis ASM International Materials Park, OH 1993 639Google Scholar
10Somekawa, H.Mukai, T.: Effect of grain size and texture on fracture toughness in magnesium and magnesium alloy in Magnesium Technology edited by A.A. Luo, N.R. Neelameggham, and R.S. Beals The Minerals, Metals and Materials Society Warrendale, PA 2006 395Google Scholar
11Armstrong, R., Codd, I., Douthwaite, R.M.Petch, N.J.: The plastic deformation of polycrystalline aggregates. Philos. Mag. A 7, 45 1962CrossRefGoogle Scholar
12Mukai, T., Yamanoi, M., Watanabe, H., Ishikawa, K.Higashi, K.: Effect of grain refinement on tensile ductility in ZK60 magnesium alloy under dynamic loading. Mater. Trans. 42, 1177 2001CrossRefGoogle Scholar
13Chapman, J.A.Wilson, D.V.: The room-temperature ductility of fine-grain magnesium. J. Inst. Metals 39, 1962–1963 2001Google Scholar
14Mukai, T., Yamanoi, M., Watanabe, H.Higashi, K.: Ductility enhancement in AZ31 magnesium alloy by controlling its grain structure. Scripta Mater. 45, 89 2001CrossRefGoogle Scholar
15Agnew, S.R., Horton, J.A., Lillo, T.M.Brown, D.W.: Enhanced ductility in strongly textured magnesium produced by equal channel angular processing. Scripta Mater. 50, 377 2004CrossRefGoogle Scholar
16Kim, W.J., An, C.W., Kim, Y.S.Hong, S.I.: Mechanical properties and microstructures of an AZ61 Mg alloy produced by equal channel angular pressing. Scripta Mater. 47, 39 2002CrossRefGoogle Scholar
17Lin, H.K., Huang, J.C.Langdon, T.G.: Relationship between texture and low temperature superplasticity in an extruded AZ31 Mg alloy processed by ECAP. Mater. Sci. Eng., A 402, 250 2005CrossRefGoogle Scholar
18Kim, H.K.Kim, W.J.: Microstructural instability and strength of an AZ31 Mg alloy after severe plastic deformation. Mater. Sci. Eng., A 385, 300 2004CrossRefGoogle Scholar
19Kim, H.K., Lee, Y.L.Chung, C.S.: Fatigue properties of a fine-grained magnesium alloy produced by equal channel angular pressing. Scripta Mater. 52, 473 2004CrossRefGoogle Scholar
20Mabuchi, M., Ameyama, K., Iwasaki, H.Higashi, K.: Low temperature superplasticity of AZ91 magnesium alloy with non-equilibrium grain boundaries. Acta Mater. 47, 2047 1999CrossRefGoogle Scholar
21Chuvildeev, V.N., Nieh, T.G., Gryaznov, M.Y., Sysoev, A.N.Kopylov, I.: Low temperature superplasticity and internal friction in microcrystalline Mg alloys processed by ECAP. Scripta Mater. 50, 861 2004CrossRefGoogle Scholar
22Matsubara, K., Miyahara, Y., Horita, Z.Langdon, T.G.: Developing superplasticity in a magnesium alloy through combination of extrusion and ECAP. Acta Mater. 51, 3073 2003CrossRefGoogle Scholar
23Watanabe, H., Mukai, T., Ishikawa, K.Higashi, K.: Low temperature superplasticity of a fine-grained ZK60 magnesium alloy processed by equal-channel-angular extrusion. Scripta Mater. 46, 851 2002CrossRefGoogle Scholar
24Somekawa, H., Singh, A.Mukai, T.: Deformation structure after fracture toughness test of Mg-Al-Zn alloys processed by equal-channel-angular extrusion. Philos. Mag. Lett. 86, 195 2006CrossRefGoogle Scholar
25Somekawa, H., Osawa, Y.Mukai, T.: Effect of solid-solution strengthening on fracture toughness in extruded Mg-Zn alloys. Scripta Mater. 55, 593 2006CrossRefGoogle Scholar
26Somekawa, H.Mukai, T.: Fracture toughness in ultra fine-grained magnesium alloy. Mater. Sci. Forum 503–504, 155 2006CrossRefGoogle Scholar
27Somekawa, H.Mukai, T.: Fracture toughness in Mg-Al-Zn alloy processed by equal-channel-angular extrusion. Scripta Mater. 54, 633 2006CrossRefGoogle Scholar
28 ASTM E399 Standard Test Method for Plane-Strain Fracture Toughness of Metallic Materials (American Society for Testing and Materials, West Conshohocken, PA, 2001)Google Scholar
29Higashi, K., Ohnishi, T., Komatsu, K., Nakatani, Y.: Evaluation of fracture toughness of 5083 and 7075 alloys by stretched zone analysis. J. Jpn. Inst. Light Metals 31, 720 1981CrossRefGoogle Scholar
30Ohira, T.Kishi, T.: Effect of iron content on fracture toughness and cracking processes in high strength Al-Zn-Mg-Cu alloy. Mater. Sci. Eng., A 78, 9 1986Google Scholar
31Barnett, M.R., Keshavarz, Z., Beer, A.G., Atwell, D.: Influence of grain size on the compressive deformation of wrought Mg-3Al-1Zn. Acta Mater. 52, 5093 2004CrossRefGoogle Scholar
32Horita, Z., Furukawa, M., Nemoto, M.Langdon, T.G.: Development of fine grained structures using severe plastic deformation. Mater. Sci. Technol. 16, 1239 2000CrossRefGoogle Scholar
33Takara, A., Nishikawa, Y., Watanabe, H., Somekawa, H., Mukai, T.Higashi, K.: Secondary processing of AZ31 magnesium alloy concomitant with grain growth or dynamic recrystallization. Mater. Trans. 45, 2377 2004CrossRefGoogle Scholar
34Yang, X., Miura, H., Sakai, T.: Dynamic evolution of new grains in magnesium alloy AZ31 during hot deformation. Mater. Trans. 44, 197 2003CrossRefGoogle Scholar
35Walls, A.A.: Unstable crack propagation in metals: Cleavage and fast fracture in Crack Propagation Symposium Proceeding Cranfield, College of Aeronautics England 1, 210 1961Google Scholar
36Watanabe, H., Mukai, T., Sugioka, M., Ishikawa, K.: Elastic and damping properties from room temperature to 673 K in an AZ31 magnesium alloy. Scripta Mater. 51, 291 2004CrossRefGoogle Scholar
37Reed-Hill, R.E.: A study of the {10-11} and {10-13} twinning modes in magnesium. Tran. Metall. Soc AIME 218, 554 1960Google Scholar
38Yoshinaga, H.Horiuchi, R.: Deformation mechanisms in magnesium single crystals compressed in the direction parallel to hexagonal axis. Mater. Trans., JIM 4, 1 1963CrossRefGoogle Scholar
39Nave, M.D.Barnett, M.R.: Microstructures and textures of pure magnesium deformed in plane-strain compression. Scripta Mater. 51, 881 2004CrossRefGoogle Scholar
40Reed-Hill, R.E.Robertson, W.D.: Additional models of deformation twinning in magnesium. Acta Mater. 5, 717 1957CrossRefGoogle Scholar
41Partridge, P.G.: The crystallography and deformation modes of hexagonal close-packed metals. Metall. Rev. 12, 169 1967CrossRefGoogle Scholar
42Yoo, M.H.: Slip, twinning and fracture in hexagonal close-packed metals. Metall. Mater. Trans. A 12, 409 1981CrossRefGoogle Scholar
43Yang, P., Yu, Y., Chen, L.Mao, W.: Experimental determination and theoretical prediction of twin orientations in magnesium alloy AZ31. Scripta Mater. 50, 1163 2004CrossRefGoogle Scholar
44Meyers, M.A., Vohringer, O.Lubarda, V.A.: Then onset of twinning in metals: A constitutive description. Acta Mater. 49, 4025 2001CrossRefGoogle Scholar
45Wosiewicz, B.C.Backofen, W.A.: Plasticity of magnesium crystals. Trans. Metall. Soc. AIME 239, 1422 1967Google Scholar
46Reed-Hill, R.E.Robertson, W.D.: The crystallographic characteristic of fracture in magnesium single crystals. Acta Mater. 5, 728 1957CrossRefGoogle Scholar
47Koike, J.Ohyama, R.: Geometrical criterion for the activation of prismatic slip in AZ61 Mg alloy sheets deformed at room temperature. Acta Mater. 53, 1963 2005CrossRefGoogle Scholar
48Agnew, S.R., Tome, C.N., Brown, D.W., Holden, T.M.Vogel, S.C.: Study of slip mechanisms in a magnesium alloy by neutron diffraction and modeling. Scripta Mater. 48, 1003 2003CrossRefGoogle Scholar
49Styczynski, A., Hartig, C., Bohlen, J.Letzing, D.: Cold rolling textures in AZ31 wrought magnesium alloy. Scripta Mater. 50, 943 2004CrossRefGoogle Scholar
50Koike, J., Kobayashi, T., Mukai, T., Watanabe, H., Suzuki, M., Maruyama, K.Higashi, K.: The activity of non-basal slip system and dynamic recovery at room temperature in fine-grained AZ31B magnesium alloys. Acta Mater. 51, 2055 2003CrossRefGoogle Scholar
51Kobayashi, T., Koike, J., Yoshida, Y., Kamado, K., Suzuki, M., Maruyama, K.Kojima, Y.: Grain size dependence of active slip systems in an AZ31 magnesium alloy. J. Jpn. Inst. Metals 67, 149 2003CrossRefGoogle Scholar
52Koike, J., Ohyama, R., Kobayashi, T., Suzuki, M.Maruyama, K.: Grain-boundary sliding in AZ31 magnesium alloys at room temperature to 523 K. Mater. Trans. 44, 445 2003CrossRefGoogle Scholar
53Somekawa, H.Mukai, T.: Effect of texture on fracture toughness in extruded AZ31 magnesium alloy. Scripta Mater. 53, 541 2005Google Scholar
54Agnew, S.R., Mehrotra, P., Lillo, T.M., Stoica, G.M.Liaw, P.K.: Texture evolution of five wrought magnesium alloys during route A equal channel angular extrusion: Experiments and simulations. Acta Mater. 53, 3135 2005CrossRefGoogle Scholar
55Liu, Y.Wu, X.: An electron-backscattered diffraction study of the texture evolution in a coarse-grained AZ31 magnesium alloy deformed in tension at elevated temperatures. Metall. Mater. Trans. A 37, 7 2006CrossRefGoogle Scholar
56Liu, F.Baker, I.: Dislocation-grain boundary interactions in ice crystals. Philos. Mag. A 72, 15 1995CrossRefGoogle Scholar
57Wang, Y.N.Huang, J.C.: The role of twinning and untwining in yielding behavior in hot-extruded Mg-Al-Zn alloy. Acta Mater. 55, 897 2007CrossRefGoogle Scholar