Hostname: page-component-cd9895bd7-dzt6s Total loading time: 0 Render date: 2024-12-23T06:56:54.416Z Has data issue: false hasContentIssue false

Effects of warm rolling reduction on the microstructure, texture and magnetic properties of Fe–6.5 wt% Si steel

Published online by Cambridge University Press:  10 May 2016

Guojun Cai
Affiliation:
State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang, Liaoning 110819, China
Changsheng Li*
Affiliation:
State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang, Liaoning 110819, China
Ban Cai
Affiliation:
State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang, Liaoning 110819, China
Qiwen Wang
Affiliation:
State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang, Liaoning 110819, China
*
a)Address all correspondence to this author. e-mail: [email protected]
Get access

Abstract

As the core materials with excellent soft magnetic properties, Fe–6.5 wt% Si steel was fabricated by using the warm rolling process due to its extremely limited ductility and formability at room temperature. In this work, the effects of warm rolling reduction varying from 50% to 85% on the microstructure, texture, and magnetic properties of sheets were explored. The microstructure and texture evolution at the various processing steps were investigated in detail using optical microscopy, electron backscatter diffraction, and transmission electron microscopy. The results demonstrate that the finer recrystallization grains are accompanied with an increasing warm rolling reduction, and the final annealed sheets are characterized by strong α-fiber and γ-fiber textures. Accordingly, on the whole, as the increase of warm rolling reductions, the values of magnetic induction (B8, B50) in the final annealed sheets increase sharply up to a maximum value and then decrease to a certain value, and the values of iron loss (P15/50, P10/400) increase monotonically.

Type
Articles
Copyright
Copyright © Materials Research Society 2016 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

Kim, K.N., Pan, L.M., Lin, J.P., Wang, Y.L., Lin, Z., and Chen, G.L.: The effect of boron content on the processing for Fe–6.5wt% Si electrical steel sheets. J. Magn. Magn. Mater. 277, 331 (2004).Google Scholar
Fu, H.D., Yang, Q., Zhang, Z.H., and Xie, J.X.: Effects of precipitated phase and order degree on bending properties of an Fe-6.5 wt% Si alloy with columnar grains. J. Mater. Res. 26, 1711 (2014).Google Scholar
Ros-Yáñez, T., Ruiz, D., Barros, J., and Houbaert, Y.: Advances in the production of high-silicon electrical steel by thermomechanical processing and by immersion and diffusion annealing. J. Alloys Compd. 369, 125 (2004).Google Scholar
Li, C.S., Yang, C.L., Cai, G.J., and Wang, Q.W.: Ordered phases and microhardness of Fe–6.5% Si steel sheet after hot rolling and annealing. Mater. Sci. Eng., A 650, 84 (2016).Google Scholar
Barros, J., Ros-Yañez, T., Vandenbossche, L., Dupré, L., Melkebeek, J., and Houbaert, Y.: The effect of Si and Al concentration gradients on the mechanical and magnetic properties of electrical steel. J. Magn. Magn. Mater. 290–291, 1457 (2005).Google Scholar
Wu, Z.Y., Fan, X.A., Wang, J., Li, G.Q., Gan, Z.H., and Zhang, Z.: Core loss reduction in Fe–6.5 wt% Si/SiO2 core–shell composites by ballmilling coating and spark plasma sintering. J. Alloys Compd. 617, 21 (2014).CrossRefGoogle Scholar
Ros-Yañez, T., Houbaert, Y., Fischer, O., and Schneider, J.: Production of high silicon steel for electrical applications by thermomechanical processing. J. Mater. Process. Technol. 143–144, 916 (2003).Google Scholar
Jung, H.J. and Kim, J.R.: Influence of cooling rate on iron loss behavior in 6.5 wt% grain-oriented silicon steel. J. Magn. Magn. Mater. 353, 76 (2014).CrossRefGoogle Scholar
Liu, H.T., Li, H.Z., Li, H.L., Gao, F., Liu, G.H., Luo, Z.H., Zhang, F.Q., Chen, S.L., Cao, G.M., Liu, Z.Y., and Wang, G.D.: Effects of rolling temperature on microstructure, texture, formability and magnetic properties in strip casting Fe–6.5 wt% Si non-oriented electrical steel. J. Magn. Magn. Mater. 391, 65 (2015).Google Scholar
Liu, Y.D., Zhang, Y.D., Ren, Y., Albert, T., and Zuo, L.: In-situ annealing study of transformation of α and γ texture of interstitial-free steel sheet by high-energy x-ray diffraction. J. Iron Steel Res. Int. 20, 38 (2013).Google Scholar
Hayakawa, Y. and Kurosawa, M.: Orientation relationship between primary and secondary recrystallized texture in electrical steel. Acta Mater. 50, 4527 (2002).Google Scholar
Morawiec, A.: On abnormal growth of Goss grains in grain-oriented silicon steel. Scr. Mater. 64, 466 (2011).CrossRefGoogle Scholar
Dafé, S.S.F., Paolinelli, S.C., and Cota, A.B.: Influence of thermomechanical processing on shear bands formation and magnetic properties of a 3% Si non-oriented electrical steel. J. Mater. Sci. Technol. 323, 3234 (2011).Google Scholar
Stoyka, V., Kováč, F., Stupakov, O., and Petryshynets, I.: Texture evolution in Fe–3% Si steel treated under unconventional annealing conditions. Mater. Charact. 61, 1066 (2010).Google Scholar
Ray, R.K., Jonas, J.J., and Hook, R.E.: Cold rolling and annealing texture in low carbon and extra low carbon steels. Int. Mater. Rev. 39, 129 (1994).Google Scholar
Wang, J., Li, J., Wang, X.F., Tian, J.J., Zhang, C.H., and Zhang, S.G.: Effect of heat rate on microstructure evolution and magnetic properties of cold rolled non-oriented electrical steel. J. Iron Steel Res. Int. 17, 54 (2010).CrossRefGoogle Scholar
Bian, X.H., Zeng, Y.P., Nan, D., and Wu, M.: The effect of copper precipitates on the recrystallization textures and magnetic properties of non-oriented electrical steels. J. Alloys Compd. 588, 108 (2014).Google Scholar
Rodríguez-Calvillo, P., Houbaert, Y., Petrov, R., Kestens, L., and Colás, R.: High temperature deformation of silicon steel. Mater. Chem. Phys. 136, 710 (2012).Google Scholar
Zhang, Y.X., Xu, Y.B., Liu, H.T., Li, C.G., Cao, G.M., Liu, Z.Y., and Wang, G.D.: Microstructure, texture and magnetic properties of strip-cast 1.3% Si non-oriented electrical steels. J. Magn. Magn. Mater. 324, 3328 (2012).Google Scholar
Bernier, N., Leunis, E., Furtado, C., Putte, T.V.D., and Ban, G.: EBSD study of angular deviations from the Goss component ingrain-oriented electrical steels. Micron 54–55, 43 (2013).CrossRefGoogle ScholarPubMed
Kim, J.K., Lee, D.N., and Koo, Y.M.: The evolution of the Goss and Cube textures in electrical steel. Mater. Lett. 122, 110 (2014).Google Scholar
Xu, Y.B., Zhang, Y.X., Wang, Y., Li, C.G., Cao, G.M., Liu, Z.Y., and Wang, G.D.: Evolution of cube texture in strip-cast non-oriented silicon steels. Scr. Mater. 87, 17 (2014).Google Scholar
Ghosh, P., Chromik, R.R., Vashegi, B., and Knight, A.M.: Effect of crystallographic texture on the bulk magnetic properties of non-oriented electrical steels. J. Magn. Magn. Mater. 365, 14 (2014).Google Scholar
Wang, J.A., Zhou, B.X., Yao, M.Y., Li, Q., and Chen, W.J.: Formation and control of sharp {l00}〈021〉 texture in electrical steel. J. Iron Steel Res. Int. 13, 54 (2006).Google Scholar
Sha, Y.H., Sun, C., Zhang, F., Patel, D., Chen, X., Kalidindi, S.R., and Zuo, L.: Strong cube recrystallization texture in silicon steel by twin-roll casting process. Acta Mater. 76, 106 (2014).Google Scholar
Chen, S., Butler, J., and Melzer, S.: Effect of asymmetric hot rolling on texture, microstructure and magnetic properties in a non-grain oriented electrical steel. J. Magn. Magn. Mater. 368, 342 (2014).Google Scholar
Landgraf, F.J.G., Emura, M., Ito, K., and Carvalho, P.S.G.: Effect of plastic deformation on the magnetic properties of non-oriented electrical steels. J. Magn. Magn. Mater. 215–216, 94 (2000).Google Scholar