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Effect of SiC nanoparticles addition on the microstructures and mechanical properties of ECAPed Mg9Al–1Si alloy

Published online by Cambridge University Press:  09 January 2017

Wanhua Wang
Affiliation:
Shanxi Key Laboratory of Advanced Magnesium Based Materials, College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China; and Key Laboratory of Interface Science and Engineering in Advanced Materials, Ministry of Education, Taiyuan University of Technology, Taiyuan 030024, China
Hongxia Wang*
Affiliation:
Shanxi Key Laboratory of Advanced Magnesium Based Materials, College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China; and Key Laboratory of Interface Science and Engineering in Advanced Materials, Ministry of Education, Taiyuan University of Technology, Taiyuan 030024, China
Yiming Liu
Affiliation:
Shanxi Key Laboratory of Advanced Magnesium Based Materials, College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China; and Key Laboratory of Interface Science and Engineering in Advanced Materials, Ministry of Education, Taiyuan University of Technology, Taiyuan 030024, China
Huihui Nie
Affiliation:
Shanxi Key Laboratory of Advanced Magnesium Based Materials, College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China; and Key Laboratory of Interface Science and Engineering in Advanced Materials, Ministry of Education, Taiyuan University of Technology, Taiyuan 030024, China
Weili Cheng
Affiliation:
Shanxi Key Laboratory of Advanced Magnesium Based Materials, College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China; and Key Laboratory of Interface Science and Engineering in Advanced Materials, Ministry of Education, Taiyuan University of Technology, Taiyuan 030024, China
*
a) Address all correspondence to this author. e-mail: [email protected]
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Abstract

This study investigated the effects of 1 wt% SiC nanoparticles addition on the microstructures and mechanical properties of Mg9Al–1Si (wt%) alloy subjected to equal channel angular pressing (ECAP). Results showed that addition of SiC nanoparticles could refine matrix grain, Mg17Al12 and Mg2Si phase of as-cast alloy, but the Mg17Al12 phase still exhibited network structure and the morphology of Mg2Si phase was still Chinese-script type. During the ECAP process, network Mg17Al12 and Chinese-script shaped Mg2Si phases were partially broken down into fine particles (∼10 µm) and much finer particles (∼2 µm) respectively. In particular, these Mg17Al12 and Mg2Si particles were uniform distribution in ECAPed Mg9Al–1Si–1SiC composite. The well-distributed particles and the existence of SiC nanoparticles could promote the formation of fine DRXed grains through enhanced grain boundary pinning. During tensile testing at room temperature, ECAPed Mg9Al–1Si–1SiC composite exhibit optimal mechanical properties, the ultimate tensile strength and elongation to failure were reached to 255 MPa and 7.9%, respectively. Furthermore, at elevated temperature of 150 °C, the tensile strength and elongation to failure were considerably increased compared to an ECAPed, SiC-free Mg9Al–1Si alloy.

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Articles
Copyright
Copyright © Materials Research Society 2017 

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Footnotes

Contributing Editor: Jürgen Eckert

References

REFERENCES

Nie, K.B., Deng, K.K., Wang, X.J., Gan, W.M., Xu, F.J., Wu, K., and Zheng, M.Y.: Microstructures and mechanical properties of SiCp/AZ91 magnesium matrix nanocomposites processed by multidirectional forging. J. Alloys Compd. 622, 1018 (2015).Google Scholar
Li, J.Y., Xie, J.X., Jin, J.B., and Wang, Z.X.: Microstructural evolution of AZ91 magnesium alloy during extrusion and heat treatment. Trans. Nonferrous Met. Soc. China 22, 1028 (2012).Google Scholar
Xie, X., Shen, J., Cheng, L., Li, Y., and Pu, Y.Y.: Effects of nano-particles strengthening activating flux on the microstructures and mechanical properties of TIG welded AZ31 magnesium alloy joints. Mater. Des. 81, 31 (2015).Google Scholar
Song, S.Y., Zhou, X., Li, L., and Ma, W.M.: Numerical simulation and experimental validation of SiC nanoparticle distribution in magnesium melts during ultrasonic cavitation based processing of magnesium matrix nanocomposites. Ultrason. Sonochem. 24, 43 (2015).CrossRefGoogle ScholarPubMed
Alizadeh, R. and Mahmudi, R.: Effects of Sb addition on the modification of Mg2Si particles and high-temperature mechanical properties of cast Mg–4Zn–2Si alloy. J. Alloys Compd. 509, 9195 (2011).Google Scholar
Moon, B.G., You, B.S., and Hahn, Y.D.: Effects of aluminum and strontium content on the microstructures and mechanical properties of Mg–Al–Ca–Sr alloys. Curr. Nanosci. 10, 108 (2014).Google Scholar
Wang, H.X., Zhou, B., Zhao, Y.T., Zhou, K.K., Cheng, W.L., and Liang, W.: Effect of Si addition on the microstructure and mechanical properties of ECAPed Mg–15Al alloy. Mater. Sci. Eng., A 589, 119 (2014).CrossRefGoogle Scholar
Wang, H.X., Liang, W., Xue, J.B., Zhao, X.G., Bian, L.P., and Zhang, J.S.: Microstructure and mechanical properties of ultrafine grained Mg15Al alloy processed by equal-channel angular pressing. J. Wuhan Univ. Technol., Mater. Sci. Ed. 25, 238 (2010).Google Scholar
Nie, K.B., Wang, X.J., Hu, X.S., Xu, L., Wu, K., and Zheng, M.Y.: Microstructure and mechanical properties of SiC nanoparticles reinforced magnesium matrix composites fabricated by ultrasonic vibration. Mater. Sci. Eng., A 528, 5278 (2011).Google Scholar
Liu, S.Y., Li, W.Z., Zhu, X., and He, G.J.: Tensile properties and fracture behavior of nano-sized SiC particles reinforced AZ91D composites at elevated temperature. Rare Met. Mater. Eng. 42(4), 761 (2013).Google Scholar
Nie, K.B., Wang, X.J., Wu, K., Hu, X.S., Zheng, M.Y., and Xu, L.: Microstructure and tensile properties of micro-SiC particles reinforced magnesium matrix composites produced by semisolid stirring assisted ultrasonic vibration. Mater. Sci. Eng., A 528, 8709 (2011).Google Scholar
Deng, K.K., Wang, C.J., Shi, J.Y., Wu, Y.W., and Wu, K.: Microstructure evolution mechanism of micron particle reinforced magnesium matrix composite at room temperature. Mater. Chem. Phys. 134, 581 (2012).CrossRefGoogle Scholar
Zhou, S.S., Deng, K.K., Li, J.C., Nie, K.B., Xu, F.J., Zhou, H.F., and Fan, J.F.: Hot deformation behavior and workability characteristics of bimodal size SiCp/AZ91 magnesium matrix composite with processing map. Mater. Des. 64, 177 (2014).CrossRefGoogle Scholar
Zhou, S.S., Deng, K.K., Li, J.C., Shang, S.J., Liang, W., and Fan, J.F.: Effects of volume ratio on the microstructure and mechanical properties of particle reinforced magnesium matrix composite. Mater. Des. 63, 672 (2014).Google Scholar
Nie, K.B., Deng, K.K., Xu, F.J., Wang, X.J., and Wu, K.: Development of microstructure in submicron particles reinforced magnesium matrix composite processed by room temperature deformation. Mater. Chem. Phys. 149, 21 (2015).Google Scholar
Wang, S.Q., Liang, W., Wang, Y., Bian, L.P., and Chen, K.H.: A modified die for equal channel angular pressing. J. Mater. Process. Technol. 209, 3182 (2009).CrossRefGoogle Scholar
Nie, K.B., Wang, X.J., Wu, K., Xu, L., Zheng, M.Y., and Hu, X.S.: Processing, microstructure and mechanical properties of magnesium matrix nanocomposites fabricated by semisolid stirring assisted ultrasonic vibration. J. Alloys Compd. 509, 8664 (2011).Google Scholar
Wang, X.J., Hu, X.S., Nie, K.B., Wu, K., and Zheng, M.Y.: Hot extrusion of SiCp/AZ91 Mg matrix composites. Trans. Nonferrous Met. Soc. China 22, 1912 (2012).Google Scholar
Zhao, Y.G., Liu, X.B., Yang, Y.Y., and Bian, T.J.: Effect of SiC particle addition on microstructure of Mg2Si/Al composite. China Foundry 11, 91 (2014).Google Scholar
Wang, Z.W., Song, M., Sun, C., and He, Y.H.: Effects of particle size and distribution on the mechanical properties of SiC reinforced Al–Cu Alloy composites. Mater. Sci. Eng., A 528, 1131 (2011).CrossRefGoogle Scholar
Hagihara, K., Kinoshita, A., Sugino, Y., Yamasaki, M., Kawamura, Y., Yasuda, H.Y., and Umakoshi, Y.: Effect of long-period stacking ordered phase on mechanical properties of Mg97Zn1Y2 extruded alloy. Acta Mater. 58, 6282 (2010).CrossRefGoogle Scholar
Shang, S.J., Deng, K.K., Nie, K.B., Li, J.C., Zhou, S.S., Xu, F.J., and Fan, J.F.: Microstructure and mechanical properties of SiCp/Mg–Al–Zn composites containing Mg17Al12 phases processed by low-speed extrusion. Mater. Sci. Eng., A 610, 243 (2014).Google Scholar
Jung, J.G., Park, S.H., Yu, H., Kim, Y.M., Lee, Y.K., and You, B.S.: Improved mechanical properties of Mg–7.6Al–0.4Zn alloy through aging prior to extrusion. Scr. Mater. 93, 8 (2014).CrossRefGoogle Scholar
Guo, W., Wang, Q.D., Ye, B., Zhou, H., and Liu, J.F.: Microstructure and mechanical properties of AZ31–Mg2Si in situ composite fabricated by repetitive upsetting. Trans. Nonferrous Met. Soc. China 24, 3755 (2014).Google Scholar
Nie, K.B., Wang, X.J., Xu, L., Wu, K., Hu, X.S., and Zheng, M.Y.: Effect of hot extrusion on microstructures and mechanical properties of SiC nanoparticles reinforced magnesium matrix composite. J. Alloys Compd. 512, 355 (2012).Google Scholar
Sanaty-Zadeh, A.: Comparison between current models for the strength of particulate-reinforced metal matrix nanocomposites with emphasis on consideration of Hall-Petch effect. Mater. Sci. Eng., A 531, 112 (2012).Google Scholar
Lin, C.Y., Tsai, H.J., Chao, C.G., and Liu, T.F.: Effects of equal channel angular extrusion on the microstructure and high-temperature mechanical properties of ZA85 magnesium alloy. J. Alloys Compd. 530, 48 (2012).CrossRefGoogle Scholar