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C/C–SiC sandwich structures manufactured via liquid silicon infiltration

Published online by Cambridge University Press:  07 July 2017

Bernhard Heidenreich ,
Dietmar Koch ,
Harald Kraft  and
Yves Klett
Bernhard Heidenreich*
Affiliation:
German Aerospace Center (DLR), Institute of Structures and Design, Stuttgart, Germany
Dietmar Koch
Affiliation:
German Aerospace Center (DLR), Institute of Structures and Design, Stuttgart, Germany
Harald Kraft
Affiliation:
German Aerospace Center (DLR), Institute of Structures and Design, Stuttgart, Germany
Yves Klett
Affiliation:
University of Stuttgart, Institute of Aircraft Design, Stuttgart, Germany
*
a)Address all correspondence to this author. e-mail: [email protected]
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Abstract

In a new design approach, C/C–SiC sandwich structures have been realized via liquid silicon infiltration and in situ joining methods. In the first process step, the carbon fiber reinforced polymer preforms for the planar skin plates as well as for the core structures were manufactured via warm pressing and autoclave technique, using C fiber fabrics preimpregnated with phenolic resin. Thereby, two types of C/C–SiC core structures were used: foldcore and grid core. In the second process step, the sandwich components were pyrolyzed separately, leading to porous C/C preforms and subsequently joined to a C/C sandwich structure, using an adhesive. In the last process step, the C/C structure was infiltrated with molten Si, and the SiC matrix was built up by a chemical reaction of Si and C, leading to a permanently joined C/C–SiC sandwich structure. For mechanical characterization, sandwich specimens were manufactured and tested in 4 point bending.

Keywords

ceramiccompositeinfiltration (chemical reaction)
Type
Invited Articles
Information
Journal of Materials Research , Volume 32 , Issue 17: Focus Issue: Achieving Superior Ceramics and Coating Properties through Innovative Processing , 14 September 2017 , pp. 3383 - 3393
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Copyright
Copyright © Materials Research Society 2017 

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Footnotes

Contributing Editor: Nahum Travitzky

References

REFERENCES

Fan, H.L., Meng, F.H., and Yang, W.: Sandwich panels with Kagome lattice cores reinforced by carbon fibers. Compos. Struct. 81, 533–539 (2007). Available at: http://www.sciencedirect.com/science/article/pii/S0263822306003874 (accessed 19 August 2016).CrossRefGoogle Scholar
Kollenberg, W.: Customized Kiln furniture. Interceram 60(3–4), 208–210 (2011).Google Scholar
Van Voorhees, E.J. and Green, D.J.: Failure behavior of cellular-core ceramic sandwich composites. J. Am. Ceram. Soc. 74, 2747–2752 (1991).CrossRefGoogle Scholar
Papenburg, U.: Advanced ultra-lightweight C/SiC mirrors and opto-mechanical structures. In Proceedings Paper of the 8th World Multi-conference on Systems, Cybernetics and Informatics, SCI 2004 (2004). Available at: http://www.unibw.de (accessed 26 January 2017).Google Scholar
Fehringer, M., Andre, G., Lamarre, D., and Maeusli, D.: A jewel in ESA’s crown—GOCE and its gravity measurement systems. ESA Bull. 133, 14–23 (2008).Google Scholar
Hurwitz, F.I.: Improved fabrication of ceramic matrix composite/foam core integrated structures. In NASA Tech Briefs (2009); p. 15. Available at: https://ntrs.nasa.gov/archive/nasa/casi.ntrs.nasa.gov (accessed 27 January 2017).Google Scholar
Ostertag, R., Haug, T., Renz, R., and Zankl, W.: Process for producing sandwich structures from fibre reinforced ceramics, U.S. Patent 5,632,834, 1997.Google Scholar
Ortona, A., Pusterla, S., and Gianella, S.: An integrated assembly method of sandwich structured ceramic matrix composites. J. Eur. Ceram. Soc., 31(9), 1821–1826 (2011). doi: 10.1016/j.jeurceramsoc.2011.03.010. Available at: http://www.sciencedirect.com (accessed 14 March 2016).CrossRefGoogle Scholar
Ferrari, L., Barbat, M., Esser, B., Petkov, I., Kuhn, M., Gianell, S., Barcena, J., Jimenez, C., Francesconi, D., Liedtke, V., and Ortona, A.: Sandwich structured ceramic matrix composites with periodic cellular ceramic cores: An active cooled thermal protection for space vehicles. Compos. Struct. 154, 61–68 (2016). Available at: http://www.sciencedirect.com (accessed 24 January 2017).CrossRefGoogle Scholar
Goodman, A., Nejhad, N.G., Wright, S., and Welson, D.: T300HoneySiC: A new near-zero CTE molded C/SiC material. In Proc. SPIE 9574, Material Technologies and Applications to Optics, Structures, Components, and Sub-Systems II, 95740E (2 September 2015), SPIE CCC code: 0277-786X/15/$18 (2015). Available at: http://dx.doi.org/10.1117/12.2185638 (26 January 2017).Google Scholar
Wright, S.: SiC-SiC and C-SiC honeycomb for advanced flight structures. SBIR award 2011 (2011). Available at: https://www.sbir.gov/print/sbirsearch/detail/369329 (accessed 26 January 2017).Google Scholar
Le, C.: New Developments in Honeycomb Core Materials (Ultracor Inc., Livermore, C.A., 2002). Rev 022802. Available at: http://www-eng.lbl.gov/∼ecanderssen/moisture/Moisture_Adsorption/NewDevelopments.pdf (accessed 31 May 2013).Google Scholar
Lengowski, M.: Development of mechanical/thermal architectures and innovative structural elements for two missions of the Stuttgart Small Satellite Program. Doctoral thesis, University of Stuttgart, Institut für Raumfahrtsysteme (IRS), 2013, pp. 120–123.Google Scholar
Krenkel, W.: Development of a cost efficient process for the manufacture of CMC components. Doctoral thesis, University of Stuttgart, DLR Forschungsbericht 2000-4, 2000.Google Scholar
Heidenreich, B., Kütemeyer, M., and Koch, D.: Development of high performance ceramic brake discs for Rail, Aircraft And Road Vehicles. In Proceedings of EuroBrake, 13–15 May 2013 (FISITA, London, 2014).Google Scholar
Krenkel, W., Henke, T., and Mason, N.: In situ Joined CMC Components. In First International Conference on Ceramic and Metal Matrix Composites CMMC 1996, Key Engineering Materials, (Trans Tech Publications, Uetikon, Switzerland, 1997); pp. 313–320.Google Scholar
Kochendörfer, R. and Krenkel, W.: CMC intake ramp for hypersonic propulsion systems. In Ceramic Matrix Composites I: Design Durability and Performance, Evans, A.G. and Naslain, R., eds., Ceram. Trans., Vol. 57 (Amer. Ceramic Society, Westerville, Ohio, 1995); pp. 13–22.Google Scholar
Gottschalk, N.: Development of C/C-SiC sandwich designs based on folded structures. Thesis, University of Stuttgart, Stuttgart, Germany, 2014.Google Scholar
Klett, Y.: Design of multifunctional isometric folded structures for technical applications. Doctoral thesis, University of Stuttgart, Institute of Aircraft Design, Dr. Hut Verlag, München, 2013. ISBN 978-3-8439-1025-5.Google Scholar
Sleiman, R.: Manufacture and characterization of C/C-SiC materials for thin walled, lightweight structures. Master's thesis, University of Stuttgart, Stuttgart, Germany, 2016.Google Scholar
Hofmann, S., Öztürk, B., Koch, D., and Voggenreiter, H.: Experimental and numerical evaluation of bending and tensile behaviour of carbon-fibre reinforced SiC. Composites, Part A 43, 1877–1885 (2012).CrossRefGoogle Scholar
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