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Bulge fatigue testing of freestanding and supported gold films

Published online by Cambridge University Press:  15 January 2014

Benoit Merle  and
Mathias Göken
Benoit Merle*
Affiliation:
Department of Materials Science and Engineering, Friedrich-Alexander-University Erlangen-Nürnberg (FAU), Institute I, Martensstr. 5, D-91058 Erlangen, Germany
Mathias Göken
Affiliation:
Department of Materials Science and Engineering, Friedrich-Alexander-University Erlangen-Nürnberg (FAU), Institute I, Martensstr. 5, D-91058 Erlangen, Germany
*
a)Address all correspondence to this author. e-mail: [email protected]
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Abstract

The bulge test was used to investigate the fatigue properties of gold thin films with a thickness between 100 and 300 nm. The membranes were pressurized at a rate of 0.2 Hz up to 105 times, during which their stress and strain states were continuously recorded. Gold films on a silicon nitride substrate were cyclically loaded into tension and compression. Due to the presence of the substrate, no membrane failure was observed, but the residual stress shifted from an initially tensile state to an increasingly compressive one. Typical fatigue damage mechanisms consisting of extrusions were found in some large grains. Freestanding films were cyclically loaded in pure tension until failure occurred. The data acquired during the fatigue tests show a strong ratcheting of the films, which is indicative of cyclic plastic creep. Microstructural investigations clearly show grain boundary sliding in very thin films with columnar grains extending through the thickness.

Keywords

bulge testthin filmfatiguegold
Type
Articles
Information
Journal of Materials Research , Volume 29 , Issue 2 , 28 January 2014 , pp. 267 - 276
Copyright
Copyright © Materials Research Society 2013 

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