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Subsolidus phase equilibria of coexisting high-Tc Pb-2223 and 2212 superconductors in the (Bi, Pb)–Sr–Ca–Cu–O system under 7.5% O2

Published online by Cambridge University Press:  31 January 2011

W. Wong-Ng ,
L. P. Cook ,
F. Jiang ,
W. Greenwood ,
U. Balachandran  and
M. Lanagan
W. Wong-Ng
Affiliation:
Ceramics Division, National Institute of Standards and Technology, Gaithersburg, Maryland 20899
L. P. Cook
Affiliation:
Ceramics Division, National Institute of Standards and Technology, Gaithersburg, Maryland 20899
F. Jiang
Affiliation:
Geology Department, University of Maryland, College Park, Maryland 20742
W. Greenwood
Affiliation:
Geology Department, University of Maryland, College Park, Maryland 20742
U. Balachandran
Affiliation:
Energy Technology Division, Argonne National Laboratory, Argonne, Illinois
M. Lanagan
Affiliation:
Energy Technology Division, Argonne National Laboratory, Argonne, Illinois
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Abstract

The subsolidus phase relationships of the high-Tc 2223 superconductor in the (Bi, Pb)–Sr–Ca–Cu–O (BSCCO) system have been examined at 810–820 °C. All experiments were carried out at ambient pressure in a 7.5% O2 (92.5% Ar) atmosphere. Eleven phases were found to exist in equilibrium with the 2223 phase. These 11 phases include CuO and 10 oxide solid solutions. From among these phases, a total of 48 five-phase combinations including the 2223 and 2212 phases were investigated experimentally, and 16 equilibrium assemblages were found which define a multicomponent compositional space corresponding to the 2223 + 2212 solid-state compatibility region. The subsolidus data form a partial basis for future investigation of the Pb-2223 primary phase field.

Type
Articles
Information
Journal of Materials Research , Volume 12 , Issue 11 , November 1997 , pp. 2855 - 2865
Copyright
Copyright © Materials Research Society 1997

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