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Preparation and characterization of nanosized zirconium (hydrous) oxide particles

Published online by Cambridge University Press:  31 January 2011

Luis A. Pérez-Maqueda  and
Egon Matijević
Luis A. Pérez-Maqueda
Affiliation:
Center for Advanced Materials Processing, Clarkson University, Potsdam, New York 13699–5814
Egon Matijević*
Affiliation:
Center for Advanced Materials Processing, Clarkson University, Potsdam, New York 13699–5814
*
b)Author to whom correspondence should be addressed.
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Abstract

A method for the preparation of nanosized zirconium (hydrous) oxide particles of narrow size distribution is described. The procedure yields stable dispersions at low temperatures and short reaction times in the absence of surfactants, using inorganic zirconium salts. Crystal structure, particle size distribution, electrokinetic properties, stability, and thermal behavior of the prepared particles were investigated. Colloidal dispersions were treated with ultrasound to study their effect on the crystal structure of the calcined samples.

Type
Articles
Information
Journal of Materials Research , Volume 12 , Issue 12 , December 1997 , pp. 3286 - 3292
Copyright
Copyright © Materials Research Society 1997

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