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Mechanical alloying of Fe and V powders: Intermixing and amorphous phase formation

Published online by Cambridge University Press:  31 January 2011

B. Fultz
Affiliation:
California Institute of Technology, 138-78, Pasadena, California 91125
G. Le Caür
Affiliation:
Laboratoire de Science et Genie des Materiaux Metalliques, associe au CNRS U.A. 159, Ecole des Mines, 54042 Nancy Cedex, France
P. Matteazzi
Affiliation:
Università di Udine, Istituto di Chimica. v. Ungheria 43, 33100 Udine, Italy
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Abstract

Mössbauer spectrometry and x-ray diffractometry were used to characterize the microstructural changes that occurred during the mechanical alloying of Fe and V powders, After 3 h of essentially no interatomic intermixing, an Fe–V alloy began to form. At first the chemical composition of this alloy was highly inhomogeneous, having large variations over distance scales of less than 100 Å. After about 24 h of ball milling, the alloy homogenized and then became at least partly amorphous.

Type
Articles
Copyright
Copyright © Materials Research Society 1989

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References

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