Hostname: page-component-586b7cd67f-dlnhk Total loading time: 0 Render date: 2024-11-26T15:25:35.820Z Has data issue: false hasContentIssue false

Flow behavior and processing map of forging commercial purity titanium powder compact

Published online by Cambridge University Press:  13 April 2015

Xiaoyan Xu*
Affiliation:
State Key Laboratory of Metal Matrix Composites, Shanghai Jiao Tong University, Shanghai 200240, China
Yuanfei Han
Affiliation:
State Key Laboratory of Metal Matrix Composites, Shanghai Jiao Tong University, Shanghai 200240, China
Changfu Li
Affiliation:
Mechanical, Materials & Aerospace Engineering, Thermal Processing Technology Center, Illinois Institute of Technology, Chicago, Illinois 60616, USA
Philip Nash
Affiliation:
Mechanical, Materials & Aerospace Engineering, Thermal Processing Technology Center, Illinois Institute of Technology, Chicago, Illinois 60616, USA
Damien Mangabhai
Affiliation:
Research and Development, Cristal Metal Inc., Lockport, Illinois 60441, USA
Weijie Lu
Affiliation:
State Key Laboratory of Metal Matrix Composites, Shanghai Jiao Tong University, Shanghai 200240, China
*
a)Address all correspondence to this author. e-mail: [email protected], [email protected]
Get access

Abstract

The flow behavior of forged commercial purity (CP) titanium powder compact was studied by developing a processing map. CP titanium powder was sintered to 94% relative density, then hot compressed in a Gleeble thermal–mechanical simulator at strain rates ranging from 0.001 to 10 s−1 and deformation temperatures ranging from 600 to 800 °C. The hot forging process improved the densification to 98–99.9% and reduced the grain size from 93 to 10 µm by the occurrence of dynamic recrystallization. The fully dynamic recrystallization region is in the range of deformation temperature of 750–800 °C and strain rate of 0.001–0.01 s−1, with a power dissipation efficiency higher than 40%, determined by constructing a processing map and analyzing the volume fraction of dynamic recrystallization. This research provides a guide for powder compact forging of power metallurgy titanium by providing the hot compression parameters, which can lead to an improved microstructure and densification.

Type
Articles
Copyright
Copyright © Materials Research Society 2015 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

Lütjering, G. and Williams, J.C.: Titanium (Springer, Berlin, 2007).Google Scholar
German, R.M.: Sintering Theory and Practice (Wiley, NewYork, USA, 1996).Google Scholar
Xu, X., Nash, G.L., and Nash, P.: Sintering mechanisms of blended Ti-6Al-4V powder from diffusion path analysis. J. Mater. Sci. 49, 9941008 (2014).CrossRefGoogle Scholar
Zhang, Z.: Simulation of titanium and titanium alloy powder compact forging. Thesis, University of Waikato, Hamilton, New Zealand, 2011.Google Scholar
German, R.M.: Powder Metallurgy Science (Metal Powder Industries Federation, Princeton, 1994).Google Scholar
Mythili, R., Saroja, S., and Vijayalakshmi, M.: Study of mechanical behavior and deformation mechanism in an α–β Ti–4.4Ta–1.9Nb alloy. Mater. Sci. Eng., A 454455, 4351 (2007).Google Scholar
Prasad, Y.V.R.K., Gegel, H.L., Doraivelu, S.M., Malas, J.C., Morgan, J.T., Lark, K.A., and Barker, D.R.: Modeling of dynamic material behavior in hot deformation: Forging of Ti-6242. Metall. Trans. A 15, 18831892 (1984).Google Scholar
Prasad, Y.V.R.K. and Seshacharyulu, T.: Processing maps for hot working of titanium alloys. Mater. Sci. Eng., A 243, 8288 (1998).Google Scholar
Han, Y., Zeng, W., Qi, Y., and Zhao, Y.: Optimization of forging process parameters of Ti600 alloy by using processing map. Mater. Sci. Eng., A 529, 393400 (2011).CrossRefGoogle Scholar
Zeng, Z., Zhang, Y., and Jonsson, S.: Deformation behaviour of commercially pure titanium during simple hot compression. Mater. Des. 30, 31053111 (2009).Google Scholar
Peng, W., Zeng, W., Wang, Q., and Yu, H.: Comparative study on constitutive relationship of as-cast Ti60 titanium alloy during hot deformation based on Arrhenius-type and artificial neural network models. Mater. Des. 51, 95104 (2013).Google Scholar
Fan, X.G., Yang, H., and Gao, P.F.: Prediction of constitutive behavior and microstructure evolution in hot deformation of TA15 titanium alloy. Mater. Des. 51, 3442 (2013).Google Scholar
Momeni, A. and Abbasi, S.M.: Effect of hot working on flow behavior of Ti-6Al-4V alloy in single phase and two phase regions. Mater. Des. 31, 35993604 (2010).Google Scholar
Zhang, X.Y., Li, M.Q., Li, H., Luo, J., Su, S.B., and Wang, H.: Deformation behavior in isothermal compression of the TC11 titanium alloy. Mater. Des. 31, 28512857 (2010).CrossRefGoogle Scholar
Jia, J., Zhang, K., and Lu, Z.: Dynamic recrystallization kinetics of a powder metallurgy Ti-22Al-25Nb alloy during hot compression. Mater. Sci. Eng., A 607, 630639 (2014).Google Scholar
Metal Powder Industries Federation: Standard Test Methods for Metal Powders and Powder Metallurgy Products (Metal Powder Industries Federation, Princeton, 1985).Google Scholar
Svoboda, J. and Riedel, H.: Pore-boundary interactions and evolution equations for the porosity and the grain size during sintering. Acta Metall. Mater. 40(11), 28292840 (1992).Google Scholar
Kang, S.L.: Sintering: Densification, Grain Growth & Microstructure (Elsevier Butterworth-Heinemann, Burlington, UK, 2005).Google Scholar
Xu, X. and Nash, P.: Sintering mechanisms of Armstrong prealloyed Ti-6Al-4V powders. Mater. Sci. Eng., A 607, 409416 (2014).Google Scholar
Sellars, C.M. and McTegart, W.J.: On the mechanism of hot deformation. Acta Metall. 14, 11361138 (1966).Google Scholar
Zener, C. and Hollomon, J.H.: Effect of strain rate upon plastic flow of steel. J. Appl. Phys. 15, 2232 (1944).Google Scholar
Zeng, Z., Jonsson, S., and Zhang, Y.: Constitutive equations for pure titanium at elevated temperatures. Mater. Sci. Eng., A 505, 116119 (2009).Google Scholar
Frost, H.J. and Ashby, M.F.: Deformation Mechanism Maps (Pergamon Press, Oxford, 1982).Google Scholar
Tanaka, H., Yamada, T., Sato, E., and Jimbo, I.: Distinguishing the ambient-temperature creep region in a deformation mechanism map of annealed CP-Ti. Scr. Mater. 54, 121124 (2006).CrossRefGoogle Scholar
Wanjara, P., Jahazi, M., Monajati, H., Yue, S., and Immarigeon, J-P.: Hot working behavior of near-α alloy IMI834. Mater. Sci. Eng., A 396, 5060 (2005).Google Scholar
Sheppard, T. and Norley, J.: Deformation characteristics of Ti-6Al-4V. Mater. Sci. Technol. 4, 903908 (1988).Google Scholar
Williams, J.C., Sommer, A.W., and Tung, P.P.: The influence of oxygen concentration on the internal stress and dislocation arrangements in α titanium. Metall. Trans. 3, 29792984 (1972).CrossRefGoogle Scholar
Weiss, I. and Semiatin, S.L.: Thermomechanical processing of alpha titanium alloys—An overview. Mater. Sci. Eng., A 263, 243256 (1999).CrossRefGoogle Scholar
Kornilov, I.I.: Effect of oxygen on titanium and its alloys. Met. Sci. Heat Treat. 15, 826829 (1973).Google Scholar
Wasz, M.L., Brotzen, F.R., McLellan, R.B., and Griffin, A.J.: Effect of oxygen and hydrogen on mechanical properties of commercial purity titanium. Int. Mater. Rev. 41(1), 112 (1996).CrossRefGoogle Scholar
Narayana Murty, S.V.S., Nageswara Rao, B., and Kashyap, B.P.: Clarification on the physical dimension of K in a constitutive equation for superplastic flow: Σ = Kεm . J. Mater. Process. Technol. 124, 259 (2002).Google Scholar
Zeigler, H.: Some extremum principles in irreversible thermodynamics with application to continuum mechanics. In Progress in Solid Mechanics, Vol. 4, Sneedon, I.N. and Hill, R. eds. (Wiley, New York, 1963); p. 63.Google Scholar
Prasad, Y.V.R.K. and Sasidhara, S.: Hot Working Guide: A Compendium of Processing Maps (ASM International, Materials Park, OH, 1997); pp. 25157.Google Scholar
Furuhara, T., Poorganji, B., Abe, H., and Maki, T.: Dynamic recovery and recrystallization in titanium alloys by hot deformation. JOM 59(1), 6467 (2007).Google Scholar
Chun, Y.B. and Hwang, S.K.: Static recrystallization of warm-rolled pure Ti influenced by microstructural inhomogeneity. Acta Metall. 56(3), 369379 (2008).Google Scholar
Narayana Murty, S.V.S., Torizuka, S., and Nagai, K.: Microstructural evolution during simple heavy warm compression of a low carbon steel: Development of a processing map. Mater. Sci. Eng., A, 410411, 319323 (2005).CrossRefGoogle Scholar
Poletti, C., Degischer, H.P., Kremmer, S., and Marketz, W.: Processing maps of Ti662 unreinforced and reinforced with TiC particles according to dynamic models. Mater. Sci. Eng., A 486, 127137 (1998).Google Scholar
Sherby, O.D., Caiigiuri, R.D., Kayali, E.S., and White, R.A.: Fundamentals of superplasticity and its applications. In Advances in Metal Processing, Burke, J.J., Mehrabian, R., and Weiss, V. eds.; Plenum Press: New York, 1981; pp. 133170.CrossRefGoogle Scholar