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Containerless solidification of YBa2Cu3O7-x in a drop tube

Published online by Cambridge University Press:  31 January 2011

V.R. Todt
Affiliation:
ACCESS e.V., Intzestraβe 5, D-5100 Aachen, Germany
G.J. Schmitz
Affiliation:
ACCESS e.V., Intzestraβe 5, D-5100 Aachen, Germany
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Abstract

YBa2Cu3O7-x was molten and resolidified by a containerless process under free-fall conditions in a drop tube. The resulting samples revealed four different microstructures originating either from a “high-temperature melt” (Tm ≥ 1550 K) or from a “low-temperature melt” (1288 K ≤ Tm ≤ 1550 K). All structures exhibited very fine, homogeneously dispersed structural constituents. One of these microstructures is not compatible with actual equilibrium phase diagrams and implies the kinetic suppression of the nucleation of both the Y2BaCuO5- and the Y2O3-phase.

Type
Articles
Copyright
Copyright © Materials Research Society 1993

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References

REFERENCES

1Murakami, M., Fujimoto, H., Oyama, T., Gotoh, S., Shiohara, Y., Koshizuka, N., and Tanaka, S., ICMC 90, High-Temperature Superconductors, Material Aspects (DGM Informationsgesellschaft, Oberursel, 1990), Vol. 1, p. 13.Google Scholar
2Sawano, K., “Preparation and properties of large bulk YBCO superconductors by quench and melt growth (QMG) process”, Proc. ISS, 90 (1990).CrossRefGoogle Scholar
3Jin, S., Tiefel, T. H., Sherwood, R. C., Davis, M. E., Dover, R. B. van, Kammlott, G.W., Fastnacht, R.A., and Keith, H.D., Appl. Phys. Lett. 52, 2074 (1988).Google Scholar
4Hirabashi, I., “Pt doping effect on melt growth of YBCO superconductor”, International Workshop on Superconductivity, Honolulu, HI, June 1992, 154157, ext. abstract.Google Scholar
5Murakami, M., “Processing of Bulk YBaCuO”, Rev. Supercon. Sci. Technol. (1992, in press).CrossRefGoogle Scholar
6Laakmann, J., Hoffmann, K., König, H., and Riillenrath, S., “Containerless processing of equiatomic Mn50Bi50 in a drop tube”, Proceedings of the VIHth Europ. Symp. on Mater, and Fluid Sciences in microgravity, Brussels, 04.92, esa special publications, in press.Google Scholar
7Folkerts, T. J., Kramer, M. J., Dennis, K. W., and McCallum, R. W., J. Mater. Res. 6, 2035 (1991).CrossRefGoogle Scholar
8Cima, M. J., Flemings, M. C., Figueredo, A. M., Nakade, M., Ishii, M., Brody, H. D., and Haggerty, J. S., J. Appl. Phys. 72 (1), 179 (1992).CrossRefGoogle Scholar