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A simple method for analysing the major volatile compounds of Asyrtiko wines subjected to pre-fermentative skin maceration

Published online by Cambridge University Press:  26 July 2007

E. SYMEOU ,
M. GALIOTOU-PANAYOTOU ,
D. KECHAGIA  and
Y. KOTSERIDIS
E. SYMEOU
Affiliation:
Department of Food Science and Technology, Agricultural University of Athens, 75, Iera Odos 11885 Athens, Greece
M. GALIOTOU-PANAYOTOU
Affiliation:
Department of Food Science and Technology, Agricultural University of Athens, 75, Iera Odos 11885 Athens, Greece
D. KECHAGIA
Affiliation:
Department of Food Science and Technology, Agricultural University of Athens, 75, Iera Odos 11885 Athens, Greece
Y. KOTSERIDIS*
Affiliation:
Department of Food Science and Technology, Agricultural University of Athens, 75, Iera Odos 11885 Athens, Greece
*
*To whom all correspondence should be addressed. Email: [email protected]
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Summary

A fast and simple method for analysing volatile compounds in Asyrtiko wines has been developed, with good reproducibility and suitability for routine analysis, and which is able to quantify many of the major odorant compounds in a single chromatographic run. The method allows satisfactory determination of fusel alcohols and their acetates, short-chain fatty acids and their ethyl esters. The linear dynamic range of the method covers the normal range of occurrence of analytes in wine, with typical r values of 0·992–0·999. Reproducibility ranges from 0·036 to 0·092 (as relative standard deviation; RSD). The method was applied for two consecutive years to wines from cv. Asyrtiko from Santorini, in order to establish the effect of pre-fermentative cryomaceration on the odorant compound levels of the resulting wines. Pre-fermentative cryomaceration significantly increased the levels of hexan-1-ol for both the vintages studied, while hexanoic acid and 2-phenylethyl acetate levels were higher in the classical vinification samples. The vintage (year) effect was important. Difference tests revealed significant differences between the samples using sensory analysis tests but preference tests did not reveal any preference for one or other treatment.

Type
Crops and Soils
Information
The Journal of Agricultural Science , Volume 145 , Issue 6 , December 2007 , pp. 577 - 585
Copyright
Copyright © Cambridge University Press 2007

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References

REFERENCES

Alvarez, I., Aleixandre, J. L., Garcia, M. J. & Lizama, V. (2006). Impact of prefermentative maceration on the phenolic and volatile compounds in Monastrell red wines. Analytica Chimica Acta 563, 109–115.Google Scholar
Bayonove, C. L. & Cordonnier, R. E. (1971). Recherches sur l'arome du Muscat. III. Etude de la fraction terpenique. Annales de Technologie Agricole 20, 347–355.Google Scholar
Bohlscheid, J. C., Wang, X. D., Mattinson, D. S. & Edwards, C. G. (2006). Comparison of headspace solid phase microextraction and XAD-2 methods to extract volatile compounds produced by Saccharomyces during wine fermentations. Journal of Food Quality 29, 1–15.Google Scholar
Bonino, M., Schellino, R., Rizzi, C., Aigotti, R., Delfini, C. & Baiocchi, C. (2003). Aroma compounds of an Italian wine (Ruche) by HS-SPME analysis coupled with GC-ITMS. Food Chemistry 80, 125–133.Google Scholar
Cabaroglu, T. & Canbas, A. (2002). The effect of skin contact on the aromatic composition of the white wine of Vitis vinifera L. cv. Muscat of Alexandria grown in Southern Anatolia. Acta Alimentaria 31, 45–55.CrossRefGoogle Scholar
Castro, Mejias R., Marin, R. N., Moreno, V. G. & Barroso, C. G. (2002). Optimisation of headspace solid-phase microextraction for analysis of aromatic compounds in vinegar. Journal of Chromatography A 953, 7–15.CrossRefGoogle Scholar
Demyttenaere, J. C. R., Dagher, C., Sandra, P., Kallithraka, S., Verhe, R. & de Kimpe, N. (2003). Flavour analysis of Greek white wine by solid-phase microextraction capillary gas chromatography-mass spectrometry. Journal of Chromatography A 985, 233–246.CrossRefGoogle ScholarPubMed
Edwards, C. G. & Beelman, R. B. (1990). Extraction and analysis of volatile compounds in white wines using Amberlite XAD-2 resin and capillary gas chromatography. Journal of Agricultural and Food Chemistry 38, 216–220.Google Scholar
Etievant, P. X. & Bayonove, C. L. (1983). Aroma components of pomaces and wine from the variety Muscat de Frontignan. Journal of the Science of Food and Agriculture 34, 393–403.Google Scholar
Etievant, P. X. (1991). Wine. In Volatile Compounds in Foods and Beverages (Ed. Maarse, H.), pp. 483–533. New York: Marcel Dekker.Google Scholar
Etievant, P. X. (1996). Artifacts and contaminants in the analysis of food flavor. Critical Reviews in Food Science and Nutrition 36, 733–745.CrossRefGoogle ScholarPubMed
Ferreira, V., Sharman, M., Cacho, J. F. & Dennis, J. (1996). New and efficient microextraction/solid-phase extraction method for the gas chromatographic analysis of wine volatiles. Journal of Chromatography A 731, 247–259.Google Scholar
Ferreira, V., Lopez, R., Escudero, A. & Cacho, J. F. (1998). Quantitative determination of trace and ultratrace flavour active compounds in red wines through gas chromatographic–ion trap mass spectrometric analysis of microextracts. Journal of Chromatography A 806, 349–354.Google Scholar
Guth, H. (1997). Quantitation and sensory studies of character impact odorants of different white wine varieties. Journal of Agricultural and Food Chemistry 45, 3027–3032.CrossRefGoogle Scholar
Jackson, R. S. (2002). Wine Tasting: A Professional Handbook. Food Science and Technology International Series. London: Academic Press.Google Scholar
Kotseridis, Y. & Baumes, R. (2000). Identification of impact odorants in Bordeaux red grape juice, in the commercial yeast used for its fermentation and in the produced wine. Journal of Agricultural and Food Chemistry 48, 400–406.CrossRefGoogle ScholarPubMed
Larmond, E. (1969). Méthodes d'Appréciation Sensorielle des Aliments en Laboratoire. Ottawa, Canada: Ministère de l'Agriculture du Canada.Google Scholar
Lopez, R., Anzar, M., Cacho, J. & Ferreira, V. (2002). Determination of minor and trace volatile compounds in wine by solid-phase extraction and gas chromatography with mass spectrometric detection. Journal of Chromatography A 966, 161–177.CrossRefGoogle ScholarPubMed
Nykänen, L. (1986). Formation and occurrence of flavor compounds in wine and distilled alcoholic beverages. American Journal of Enology and Viticulture 37, 84–96.Google Scholar
OIV (1990). Recueil des Méthodes Internationales d'Analyse des Vins et des MoÛts. Paris, France: Office International de la Vigne et du Vin.Google Scholar
Ortega, C., Lopez, R., Cacho, J. & Ferreira, V. (2001). Fast analysis of important wine volatile compounds. Development and validation of a new method based on gas-chromatographic–flame ionization detection analysis of dichloromethane microextracts. Journal of Chromatography A 923, 205–214.Google Scholar
Ortega-Heras, M., Gonzalez-SanJose, M. L. & Beltran, S. (2002). Aroma composition of wine studied by different extraction methods. Anlytica Chimica Acta 458, 85–93.Google Scholar
Palomo, E. S., Perez-Coello, M. S., Diaz-Maroto, M. C., Gonzalez-Vinas, M. A. & Cabezudo, M. D. (2006). Contribution of free and glycosidically-bound volatile compounds to the aroma of muscat ‘a petit grains’ wines and effect of skin contact. Food Chemistry 95, 279–289.Google Scholar
Peinado, R. A., Moreno, J., Bueno, J. E., Moreno, J. A. & Mauricio, J. C. (2004). Comparative study of aromatic compounds in two young white wines subjected to pre-fermentative cryomaceration. Food Chemistry 84, 585–590.Google Scholar
Rapp, A. (1988). Volatile flavour of wine: correlation between instrumental analysis and sensory perception. Nahrung 42, 351–363.3.3.CO;2-U>CrossRefGoogle Scholar
Rapp, A. & Knipser, W. (1980). Determination of polar analytes in aqueous matrices by purge and trap. Chromatographia 13, 698–702.Google Scholar
Rapp, A. & Mandery, H. (1986). Wine aroma. Experentia 42, 873–884.CrossRefGoogle Scholar
Ribereau-Gayon, P., Dubourdieu, D., Doneche, B. & Lonvaud, A. (2000). The Microbiology of Wine and Vinifications. Handbook of Enology, Vol. 1. Chichester, UK: John Wiley & Sons.Google Scholar
Selli, S., Canbas, A., Cabaroglu, T., Erten, H. & Gunata, Z. (2006 a). Aroma components of cv. Muscat of Bornova wines and influence of skin contact treatment. Food Chemistry 94, 319–326.CrossRefGoogle Scholar
Selli, S., Canbas, A., Cabaroglu, T., Erten, H., Lepoutre, J. P. & Gunata, Z. (2006 b). Effect of skin contact on the free and bound aroma compounds of the white wine of Vitis vinifera L. cv Narince. Food Control 17, 75–82.Google Scholar
Strauss, C. R., Wilson, B. & Williams, P. J. (1988). Novel monoterpene diols and diol glycosides on Vitis vinifera grapes. Journal of Agricultural and Food Chemistry 36, 569–573.Google Scholar
Vas, G., Gal, L., Harangi, J., Dobo, A. & Vekey, K. (1998). Determination of volatile aroma compounds of Blaufrankisch wines extracted by solid-phase microextraction. Journal of Chromatographic Science 36, 505–510.Google Scholar
Williams, P. J., Strauss, C. R. & Wilson, B. (1980). Hydroxylated linalool derivatives as precursors of volatile monoterpenes of Muscat grapes. Journal of Agricultural and Food Chemistry 28, 766–771.Google Scholar
Wilson, B., Strauss, C. R. & Williams, P. J. (1984). Changes in free and glycosidically-bound monoterpenes in developing Muscat grapes. Journal of Agricultural and Food Chemistry 32, 919–924.CrossRefGoogle Scholar
Wilson, B., Strauss, C. R. & Williams, P. J. (1986). The distribution of free and glycosidically-bound monoterpenes among skin, juice and pulp fractions of some white grape varieties. American Journal of Enology and Viticulture 37, 107–111.Google Scholar