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Design of a high-pressure and high-temperature cell for operando X-ray absorption spectroscopy in heterogeneous catalysis
Published online by Cambridge University Press: 18 January 2011
Abstract
A new X-ray absorption cell dedicated to in situ and operando experiments in heterogeneous catalysis has been built and tested. It allows measurement of X-ray absorption spectroscopy (XAS) spectra in transmission mode under the flow of various gas mixtures at elevated temperatures (600°C) and pressures (50 bar). The working conditions are representative of phenomena that take place in fixed bed reactors.
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- Copyright © Diamond Light Source Ltd 2011
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