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Anomalies in the Ethylene Glycol Solvation Technique Used in X-Ray Diffraction

Published online by Cambridge University Press:  01 January 2024

G. W. Kunze
G. W. Kunze*
Affiliation:
Agricultural and Mechanical College of Texas, USA
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Abstract

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X-ray diffraction results are presented to show that some montmorillonites will not retain two layers of ethylene glycol in the interlayer space when dried under atmospheric conditions. Diffraction data obtained from such samples of montmorillonite may erroneously be attributed to mixed layer minerals. Studies have shown however that this difficulty may largely be overcome by initially saturating the sample with ethylene glycol by the vaporization technique described, after which the sample is placed in a saturated atmosphere of ethylene glycol for a period of 12–24 hours to come to equilibrium and then irradiated.

Type
Article
Information
Clays and Clay Minerals (National Conference on Clays and Clay Minerals) , Volume 3 , February 1954 , pp. 88 - 93
Copyright
Copyright © The Clay Minerals Society 1954

Footnotes

Contribution from the Texas Agr. Exp. Sta., College Station, Texas, as Technical Article No. 2111.

References

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