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Two-Crystal X-Ray Spectrometer Attachment

Published online by Cambridge University Press:  06 March 2019

Leonid V. Azároff*
Affiliation:
Illinois institute of Technology, Chicago, Illinois
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Abstract

A two-crystal spectrometer that makes full use of conventional diffractometet: or spectrometer motions has been constructed so that it can be easily attached to a commercial instrument. The requisite degree of parallelism of the two crystalrotation axes is maintained by keeping both parallel to a single ground surface. Special alignment aids have been constructed to facilitate the rapid alignment of the instrument, which can be operated manually in 1″ intervals or used for automatic scanning in steps of 0.01°. Some guide lines for comparing the relative performance of spectrometers in X-ray absorption spectroscopy are suggested.

Type
Research Article
Copyright
Copyright © International Centre for Diffraction Data 1965

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References

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