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Problems in the Temperature Calibration of an X-Ray Diffractometer Furnace*

Published online by Cambridge University Press:  06 March 2019

F.A. Mauer  and
L.H. Bolz
F.A. Mauer
Affiliation:
National Bureau of Standards, Washington, D.C.
L.H. Bolz
Affiliation:
National Bureau of Standards, Washington, D.C.
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Abstract

Tests were carried out with an X-ray diffractometer furnace to determine the temperature variations from point to point in the specimen and the correction to be applied to thermocouple readings. It was found that, under the conditions of the tests, temperature corrections depend on the preparation and properties of the sample. Calibration curves for two standards are given to illustrate this point, and suggestions for improving temperature measurements are made.

Type
Research Article
Information
Advances in X-Ray Analysis , Volume 5: Tenth Annual Conference on Applications of X-ray Analysis, August 7-9, 1961 , 1961 , pp. 229 - 237
Copyright
Copyright © International Centre for Diffraction Data 1961

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Footnotes

*

This work was supported by the Aeronautical Research Laboratory, Office of Aerospace Resarch, Wright — Patterson Air Force Base, Ohio, United States Air Force.

References

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