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Electron Microprobe Analysis of Highly Radioactive Samples

Published online by Cambridge University Press:  06 March 2019

V. G. Scotti ,
J. M. Johnson  and
R. T. Cunningham
V. G. Scotti
Affiliation:
Pratt and Whitney, Aircraft (CANEL) Middletown, Connecticut
J. M. Johnson
Affiliation:
Pratt and Whitney, Aircraft (CANEL) Middletown, Connecticut
R. T. Cunningham
Affiliation:
Pratt and Whitney, Aircraft (CANEL) Middletown, Connecticut
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Abstract

An electron microprobe analyzer shielded and modified to accept for analysis radioactive samples reading up to 100 R/hr is described. The following features will be illustrated and discussed: (1) biological shielding, (2) detector shielding, (3) sample transfer system, (4) remote sample loading and focusing system, (5) laboratory layout, and (6) experimental results.

Type
Research Article
Information
Advances in X-Ray Analysis , Volume 9: Fourteenth Annual Conference on Applications of X-ray Analysis, August 25-27, 1965 , 1965 , pp. 314 - 322
Copyright
Copyright © International Centre for Diffraction Data 1965

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References

1. Bradbury, B. T., Demajnt, J. T., Martin, P. M., and Poole, D. M., “Electron Probe Microanalysis of Irradiated UO2,” AERE-R-4845, 1965.Google Scholar
2. Fornwalt, D. E., Gourley, B. R., and Manzione, A. V., “A study of the Compatibility of Selected Refractory Metals with Various Ceramic Insulation Materials,” CNLM-S942, presented at Electron Microprobe Symposium of Electrochemical Society Meeting, Washington, D.C., October, 1964.Google Scholar
3. Ziebold, T. O. and Ogilvie, R. E., Anal. Chem. 36: 322 (1964).Google Scholar