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An Automated X-Ray Diffractometer for Detection and Identification of Minor Phases
Published online by Cambridge University Press: 06 March 2019
Extract
In the preceding volume in this series, we described a stepping motor automation package for XRD data acquisition, based on the Apple microcomputer with an interface card that produces the stepping motor pulses and counts X-ray pulses from the normal X-ray detector and amplifier. We are presently using the system to automate a General Electric XRD-5 diffractometer mechanism, by replacing the original synchronous motor with the stepping motor, and installing 10:1 reduction gear instead of the chain drive to drive the double worm gears. This gives 2500 steps of the motor per degree two theta. Motor pulses are counted by a small machine language routine which also handles accelerating the mechanism when slewing over long angular ranges.
- Type
- IV. XRD Applications and Automation
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- Copyright © International Centre for Diffraction Data 1982