Hostname: page-component-586b7cd67f-dlnhk Total loading time: 0 Render date: 2024-11-23T12:35:16.990Z Has data issue: false hasContentIssue false
  • English
  • Français

The X-Ray Investigation of Preprecipitation in Supersaturated Solid Solutions

Published online by Cambridge University Press:  06 March 2019

A. Lutts
A. Lutts*
Affiliation:
Centre National de Recherches Métallurgiques, Liège, Belgium
Get access

Abstract

This paper briefly traces the study of the preprecipitation or cold-aging stage of the decomposition of supersaturated solutions by means of diffuse scattering of X-rays.

This part of the overall precipitation process is of considerable practical as well as theoretical interest because it is during preprecipitation that changes in many physical and mechanical properties take place without the formation of a precipitate phase.

Examples will be given to show the types of zones encountered during this stage in various age-hardening alloys. These will attempt to illustrate the contribution which the study of diffuse scattering of X-rays, guided by present-day concepts of crystal imperfections, has made toward a better understanding of the precipitation process in alloys.

Type
Research Article
Information
Advances in X-Ray Analysis , Volume 6: Eleventh Annual Conference on Applications of X-ray Analysis, August 8-10, 1962 , 1962 , pp. 25 - 42
Copyright
Copyright © International Centre for Diffraction Data 1962

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1. Schmidt, E. and Wasserman, E., Naturwissenschaften 14: 980, 1926.Google Scholar
2. Fraenkel, W. and Seng, R., Z. Metallkunde 12: 225, 1920.Google Scholar
3. Merica, P. D., Wallenberg, R. G., and Scott, H., U.S. Bureau of Standards Scientific Paper 347, 1919; AIME Tram. 64: 41, 1921.Google Scholar
4. Merica, P. D., AIME Trans. 99: 13, 1932.Google Scholar
5. Guinier, A., Compt. rend, 206: 1641, 1938.Google Scholar
6. Guinier, A., Nature 142: 569, 1938.Google Scholar
7. Preston, G. D., Nature 142: 570, 1938.Google Scholar
8. Guinier, A., J. Metals 8: 673, 1956.Google Scholar
9. Guinier, A., Théorie et technique de la radiocrhtallographie, Dunod, Paris, 1956.Google Scholar
10. Geisler, A. H. and Hill, J. K., Acta Cryst. 1: 238, 1948.Google Scholar
11. Jagodzinski, H., Z. Metallkunde 46: 491, 1955.Google Scholar
12. Compton, A. H. and Allison, S. K., X-rays in Theory and Experiment, D. Van Nostrand Co., Inc., Princeton, N. J., 1935.Google Scholar
13. Lambert, M., Thesis, University of Paris, 1958.Google Scholar
14. Guinier, A., Ann. phys. 12: 161, 1939.Google Scholar
15. Ewald, P. P., Proc. Phys. Soc. (London) 44: 257, 1914.Google Scholar
16. Hardy, H. K. and Heal, T. J., “Report on Precipitation,” Prog. Metal Phys. 5, 1954.Google Scholar
17. Preston, G. D., Proc Roy. Sac. (London) A 167: 526, 1938.Google Scholar
18. Preston, G. D., Phil. Mag. 26: 855, 1938.Google Scholar
19. Geisler, A. H., Barrett, C. S., and Mehl, R. F., AIME Trans. 152: 182, 1943.Google Scholar
20. Barrett, C. S. and Geisler, A. H., J. Appl. Phys. 11: 733, 1940.Google Scholar
21. Guy, A. G., Barrett, C. S., and Mehl, R. F., AIME Trans. 175: 216, 1948.Google Scholar
22. Geisler, A. H. and Mehl, R. F., AIME Trans. 143: 134, 1941.Google Scholar
23. Silcock, J. M., Heal, T. J., and Hardy, H. K., J. Inst. Metals 82, 1953-54, p. 239.Google Scholar
24. Foumet, G., Bull. soc. franç, minéral, et. crist. 74: 39, 1951.Google Scholar
25. Guinier, A. and Fournet, G., Small-Angle Scattering of X-rays, John Wiley & Sons, Inc., New York, 1955.Google Scholar
26. Dowling, P. H., Hendee, C. F., Kuhlin, T. R., and Parrish, W., Phillips Tech. Rev. 18: 262, 1956.Google Scholar
27. Glocker, R., Koster, W., Scherb, J., and Ziegler, G., Z. Metallkunde 43: 208, 1952.Google Scholar
28. Graf, R., Publs, sci. et tech. ministère air, No. 315, 1956.Google Scholar
29. Hardy, H. K., J. Imt. Metals 75: 707, 1948-49.Google Scholar
30. Guinier, A., “Heterogeneities in Solid Solutions,” in Solid State Physics, Vol. 9, Academic Press, Inc., New York, p. 345.Google Scholar
31. Wassermann, G. and Weerts, J., Metallwirtschaft 14: 605, 1935.Google Scholar
32. Guinier, A. and Jacquet, P., Compt. rend. 217: 22, 1943.Google Scholar
33. Guinier, A. and Jacquet, P., Rev. mét. 41: 1, 1944.Google Scholar
34. Geisler, A. H., Mallery, J. H., and Steigert, F. E., J. Metals 4: 307, 1952.Google Scholar
35. Barrett, C. S., Geisler, A. H., and Mehl, R. F., AIME Trans. 143: 134, 1941.Google Scholar
36. Guinier, A., J. phys. rad. 8(3): 124, 1942.Google Scholar
37. Guinier, A., Z. Metallkunde 43: 217, 1952.Google Scholar
38. Walker, C. B. and Guinier, A., Compt. rend. 234: 2379, 1952.Google Scholar
39. Walker, C. B., Blin, J., and Guinier, A., Compt. rend. 235: 254, 1952.Google Scholar
40. Rudman, P. S., Flinn, P. A., and Averbach, B. L., J. Appl. Phys. 24: 365, 1953.Google Scholar
41. Ziegler, G., Z. Metallkunde 43: 213, 1952.Google Scholar
42. Köster, W. and Eraumann, F., Z. Metallkunde 43: 193, 1952.Google Scholar
43. Köster, W., Steinert, H., and Scherb, J., Z. Metallkunde 43: 202, 1952.Google Scholar
44. Guinier, A., Métaux et corrosion 18: 209, 1943.Google Scholar
45. Guinier, A. and Larnbot, H., Compt. rend. 227: 74, 1948.Google Scholar
46. Lambot, H., Doctorate Thesis, University of Paris, 1950.Google Scholar
47. Lambot, H., Rev. met. 47: 709, 1950.Google Scholar
48. Lambot, H., Bull. acad. roy. soc. Belg. 26: 1609, 1950.Google Scholar
49. Cttstaing, R. and Guinier, A., Compt. rend. 229: 1146, 1949.Google Scholar
50. Castaing, R. and Guinier, A., Compt. rend. 228: 2033, 1949.Google Scholar
51. Graf, R., Compt. rend. 242: 1311, 1956; 244: 337, 1957.Google Scholar
52. Schmalzried, H. and Gerold, V., Z. Metallkunde 49: 291, 1958.Google Scholar
53. Hardy, H. K., J. Inst. Metals 79: 321, 1951.Google Scholar
54. Mehl, R. F., Rhines, F. W., and van der Steinen, K. A., Metals & Alloys 13(1): 41, 1941.Google Scholar
55. Turnbull, D., Report Bristol Conference on Defects in Crystalline Solids, 1954, 1955, p. 203.Google Scholar
56. Kauffman, J. W. and Koehler, J. S., Phys. Rev. 97: 555, 1955.Google Scholar
57. Rohner, F., J. Inst. Metals 73: 285, 1947.Google Scholar
58. Seitz, F., L'état solide, R. Stoops, Brussels, 1952, p. 405.Google Scholar
59. Lutts, A. and Lambot, H., Rev. met. 54: 775, 1957.Google Scholar
60. Lutts, A., Doctorate Thesis, University of Liege, 1960.Google Scholar
61. Lutts, A., Acta Met. 9: 577, 1961.Google Scholar
62. Panseri, C., Gatto, F., and Federighi, T., Acta Met. 6: 198, 1958.Google Scholar