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X-Ray Fluorescence Analysis of Welding Fume Particles

Published online by Cambridge University Press:  06 March 2019

Thomas P. Carsey
Thomas P. Carsey*
Affiliation:
National Institute for Occupational Safety and Health Cincinnati, Ohio 45227
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Extract

The technique of x-ray fluorescence is ideal for the analysis of metal fumes such as are produced in various welding and brazing operations. Although the constitution of welding and brazing fumes is dependent on the nature of the base metal, flux, and welding material used, they typically contain the oxides of iron, nickel, chromium, and manganese (stainless steel welding). The fumes are in the form of very small particles, usually 1.0 um, and are often agglomerated into long chains. Filter samples of these fumes, as are used in industrial hygiene monitoring, may contain 30-300 ug/filter of particles on one surface of a low-mass, 37-mm membrane filter.

Type
V. XRF Environmental Applications
Information
Advances in X-Ray Analysis , Volume 25: Thirtieth Annual Conference on Applications of X-ray Analysis, August 3-7, 1981 , 1981 , pp. 209 - 212
Copyright
Copyright © International Centre for Diffraction Data 1981

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References

1. Criteria for a Recommended Standard... Occupational Exposure to Welding, Brazing, and Thermal Cutting,” (Draft), DHHS-NIOSH (1979).Google Scholar
2. “Fumes and Gases in the Welding Environment,” American Welding Society, Miami, Florida, 1979.Google Scholar
3. Carsey, T. P., “Feasibility Study for X-ray Fluorescence Analysis of Welding and Brazing Fumeis,” submitted to national Technical Information Service (HTIS).Google Scholar
4. Semmler, R. A., Draftz, R. D., and Puretz, I., “Thin-Layer Standards for Calibration of X-ray Spectrometers,” in “X-ray Fluorescence of Environmental Samples,” Dzubay, T., Ed., Ann Arbor, 1977, p. 181.Google Scholar
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