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Use of the Dow-Developed DSC/XRD/MS in the Study of Several Model Copper-Based Catalyst Systems

Published online by Cambridge University Press:  06 March 2019

R. A. Newman ,
J. A. Blazy ,
T. G. Fawcett ,
L. F. Whiting  and
R. A. Stowe
R. A. Newman
Affiliation:
Michigan Applied Science & Technology Laboratories, The Dow Chemical Company, Midland, Michigan 48674
J. A. Blazy
Affiliation:
Michigan Applied Science & Technology Laboratories, The Dow Chemical Company, Midland, Michigan 48674
T. G. Fawcett
Affiliation:
Michigan Applied Science & Technology Laboratories, The Dow Chemical Company, Midland, Michigan 48674
L. F. Whiting
Affiliation:
Michigan Applied Science & Technology Laboratories, The Dow Chemical Company, Midland, Michigan 48674
R. A. Stowe
Affiliation:
Michigan Applied Science & Technology Laboratories, The Dow Chemical Company, Midland, Michigan 48674
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Extract

Due to the difficulty of analyzing materials at high temperatures and in reactive atmospheres, solid-state catalysts have often been developed with little knowledge of the true chemical behavior of the catalyst, except on a bulk scale. In the field of solid-state catalysis research, a great deal of time and effort is presently being spent to better characterize the chemical and physical properties which determine a particular catalyst‘s efficiency, lifetime, and selectivity. Recently, we have undertaken a study of model copper catalysts at The Dow Chemical Company in an effort to better understand the chemical and physical properties which determine the efficiency, regenerability, and lifetime of this type of solid state catalyst.

Type
IX. High Temperature and Non-Ambient Powder Diffraction Applications
Information
Advances in X-Ray Analysis , Volume 30: Thirty-Fifth Annual Conference on Applications of X-ray Analysis, August 4-8, 1986 , 1986 , pp. 493 - 502
Copyright
Copyright © International Centre for Diffraction Data 1986

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References

1. Fawcett, T.G., et. al,, “The Rapid Simultaneous Measurement of Thermal and Structural Data by a Novel DSC/XRD. Instrument”, Adv. in X-ray Analysis, 28, 227 (1885).Google Scholar
2. Crowder, C.E., et. al., “Analysis of the Thermo-Structural Behavior of Polyethylene using Simultaneous DSC/XRD”, Adv. in X-ray Analysis, 29, 315 (1986).Google Scholar
3. Blazsy, J.A., et. al., “Analysis of Multi-Phase Pharmaceuticals Using Simultaneous Differential Scanning. Calorimetry and X-ray Diffraction”, Adv. in X-ray Analysis, 29, 323 (1986).Google Scholar
4. Johnson, D.A., “Some Thermodynamic Aspects of Inorganic Chemistry”, Cambridge University Press, Appendix 5 (1968).Google Scholar